5-<(1-N,N'dietoxycarbonylhydrazino)ethyl>-3-methylthio-1,4-diphenyl-1,2,4-triazolium iodide

Base Information

Chemical Name:5-<(1-N,N'dietoxycarbonylhydrazino)ethyl>-3-methylthio-1,4-diphenyl-1,2,4-triazolium iodide
CAS No.:76116-92-2
Molecular Formula:C₂₃H₂₈N₅O₄S*I
Molecular Weight:597.477
Hs Code.:

Synonyms:5-<(1-N,N'dietoxycarbonylhydrazino)ethyl>-3-methylthio-1,4-diphenyl-1,2,4-triazolium iodide

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Chemical Property of 5-<(1-N,N'dietoxycarbonylhydrazino)ethyl>-3-methylthio-1,4-diphenyl-1,2,4-triazolium iodide

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Technology Process of 5-<(1-N,N'dietoxycarbonylhydrazino)ethyl>-3-methylthio-1,4-diphenyl-1,2,4-triazolium iodide

There total 2 articles about 5-<(1-N,N'dietoxycarbonylhydrazino)ethyl>-3-methylthio-1,4-diphenyl-1,2,4-triazolium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 56017-94-8
5-methyl-3-methylthio-1,4-diphenyl-1,2,4-triazolium iodide

: 1972-28-7,218603-74-8
diethylazodicarboxylate

: 76116-92-2
5-<(1-N,N'dietoxycarbonylhydrazino)ethyl>-3-methylthio-1,4-diphenyl-1,2,4-triazolium iodide

Guidance literature:: With potassium iodide; In N,N-dimethyl-formamide; at 100 ℃; for 0.333333h;
DOI:10.1016/S0040-4020(01)83135-5

Reference yield:

: 54211-56-2
3-methyl-1,4-diphenyl isothiosemicarbazide

: 76116-92-2
5-<(1-N,N'dietoxycarbonylhydrazino)ethyl>-3-methylthio-1,4-diphenyl-1,2,4-triazolium iodide

Guidance literature:: Multi-step reaction with 2 steps

1: POCl₃, KI / pyridine / Heating

2: 57 percent / KI / dimethylformamide / 0.33 h / 100 °C

With potassium iodide; trichlorophosphate; In pyridine; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)83135-5