methyl 6-(2,6-dimethoxyphenyl)-4-methylcyclohexa-1,4-diene-1-carboxylate

Base Information

Chemical Name:methyl 6-(2,6-dimethoxyphenyl)-4-methylcyclohexa-1,4-diene-1-carboxylate
CAS No.:1396312-41-6
Molecular Formula:C₁₇H₂₀O₄
Molecular Weight:288.343
Hs Code.:

Synonyms:methyl 6-(2,6-dimethoxyphenyl)-4-methylcyclohexa-1,4-diene-1-carboxylate

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Chemical Property of methyl 6-(2,6-dimethoxyphenyl)-4-methylcyclohexa-1,4-diene-1-carboxylate

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Technology Process of methyl 6-(2,6-dimethoxyphenyl)-4-methylcyclohexa-1,4-diene-1-carboxylate

There total 2 articles about methyl 6-(2,6-dimethoxyphenyl)-4-methylcyclohexa-1,4-diene-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 141992-10-1
2',6'-dimethoxy-1'-((E)-3-methylbuta-1,3-dienyl)benzene

: 922-67-8
propynoic acid methyl ester

: 1396312-41-6
methyl 6-(2,6-dimethoxyphenyl)-4-methylcyclohexa-1,4-diene-1-carboxylate

Guidance literature:: With hydroquinone; In dichloromethane; at 40 ℃; for 44h; under 6750680 Torr; Solvent; regioselective reaction;
DOI:10.1021/jo301203k

Reference yield: 43.0%

: 141992-10-1
2',6'-dimethoxy-1'-((E)-3-methylbuta-1,3-dienyl)benzene

: 922-67-8
propynoic acid methyl ester

: 1396312-41-6
methyl 6-(2,6-dimethoxyphenyl)-4-methylcyclohexa-1,4-diene-1-carboxylate

: 1396312-47-2
methyl 2',6'-dimethoxy-4-methyl-1',6-biphenyl-1-carboxylate

Guidance literature:: With hydroquinone; In ethanol; at 80 ℃; for 120h; under 750.075 Torr; Overall yield = 75 %; regioselective reaction;
DOI:10.1021/jo301203k