(4S,5S)-4-(2,4-Dinitro-phenylamino)-5-(2-methyl-4-phenyl-butyl)-dihydro-furan-2-one

Base Information

• Chemical Name: (4S,5S)-4-(2,4-Dinitro-phenylamino)-5-(2-methyl-4-phenyl-butyl)-dihydro-furan-2-one
• CAS No.: 119437-79-5
• Molecular Formula: C₂₁H₂₃N₃O₆
• Molecular Weight: 413.43

Synonyms:(4S,5S)-4-(2,4-Dinitro-phenylamino)-5-(2-methyl-4-phenyl-butyl)-dihydro-furan-2-one

Chemical Property of (4S,5S)-4-(2,4-Dinitro-phenylamino)-5-(2-methyl-4-phenyl-butyl)-dihydro-furan-2-one

Chemical Property:

Purity/Quality:

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Technology Process of (4S,5S)-4-(2,4-Dinitro-phenylamino)-5-(2-methyl-4-phenyl-butyl)-dihydro-furan-2-one

There total 2 articles about (4S,5S)-4-(2,4-Dinitro-phenylamino)-5-(2-methyl-4-phenyl-butyl)-dihydro-furan-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,4-Dinitrofluorobenzene (70-34-8,65727-75-5) + (4S,5S)-4-Amino-5-(2-methyl-4-phenyl-butyl)-dihydro-furan-2-one (119437-78-4) → (4S,5S)-4-(2,4-Dinitro-phenylamino)-5-(2-methyl-4-phenyl-butyl)-dihydro-furan-2-one (119437-79-5)

Guidance literature:

With TEA; In diethyl ether; for 2h; Ambient temperature;

DOI:10.1021/jo9718455

Reference yield:

2,4-Dinitrofluorobenzene (70-34-8,65727-75-5) + theonellamide F (119455-31-1) → (4S,5S)-4-(2,4-Dinitro-phenylamino)-5-(2-methyl-4-phenyl-butyl)-dihydro-furan-2-one (119437-79-5)

Guidance literature:

Yield given. Multistep reaction;

DOI:10.1021/ja00189a035

Reference yield:

(4S,5S)-4-(2,4-Dinitro-phenylamino)-5-(2-methyl-4-phenyl-butyl)-dihydro-furan-2-one (119437-79-5) → (3S,4S)-3-(2,4-Dinitro-phenylamino)-4-hydroxy-6-methyl-8-phenyl-octanoic acid (119437-80-8)

Guidance literature:

With potassium carbonate; In methanol; for 1h; Yield given; Ambient temperature;

DOI:10.1021/ja00189a035

upstream raw materials:

2,4-Dinitrofluorobenzene

theonellamide F

(4S,5S)-4-Amino-5-(2-methyl-4-phenyl-butyl)-dihydro-furan-2-one

Downstream raw materials:

(3S,4S)-3-(2,4-Dinitro-phenylamino)-4-hydroxy-6-methyl-8-phenyl-octanoic acid

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