methyl L-alanyl-L-phenylalanine trifluoroacetate

Base Information

Chemical Name:methyl L-alanyl-L-phenylalanine trifluoroacetate
CAS No.:87892-68-0
Molecular Formula:C₂HF₃O₂*C₁₃H₁₈N₂O₃
Molecular Weight:364.321
Hs Code.:

Synonyms:methyl L-alanyl-L-phenylalanine trifluoroacetate

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Chemical Property of methyl L-alanyl-L-phenylalanine trifluoroacetate

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Technology Process of methyl L-alanyl-L-phenylalanine trifluoroacetate

There total 5 articles about methyl L-alanyl-L-phenylalanine trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 2280-66-2
N-tert-butyloxycarbonylalanylphenylalanine methyl ester

: 76-05-1
trifluoroacetic acid

: 87892-68-0
methyl L-alanyl-L-phenylalanine trifluoroacetate

Guidance literature:: In dichloromethane; for 0.5h; Ambient temperature;
DOI:10.1016/S0040-4039(98)01878-4

Reference yield:

: 7524-50-7
methyl (2S)-2-amino-3-phenylpropanoate hydrochloride

: 87892-68-0
methyl L-alanyl-L-phenylalanine trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1: EDC, HOBt, NMM / CH₂Cl₂ / 48 h / 0 - 20 °C

2: 100 percent / CH₂Cl₂ / 0.5 h / Ambient temperature

With 4-methyl-morpholine; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In dichloromethane;
DOI:10.1016/S0040-4039(98)01878-4

Reference yield:

: 19460-86-7
(N-methyl)-L-phenylalanine methyl ester hydrochloride

: 87892-68-0
methyl L-alanyl-L-phenylalanine trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1: BOP, triethylamine / acetonitrile / 2 h

2: methylene chloride / 0.5 h

With dichloromethane; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; In acetonitrile;
DOI:10.1016/0040-4020(81)85016-8