2,4-dibromo-3,6-dimethoxyaniline

Base Information

• Chemical Name: 2,4-dibromo-3,6-dimethoxyaniline
• CAS No.: 1160574-43-5
• Molecular Formula: C₈H₉Br₂NO₂
• Molecular Weight: 310.973

Synonyms:2,4-dibromo-3,6-dimethoxyaniline

Chemical Property of 2,4-dibromo-3,6-dimethoxyaniline

Chemical Property:

Purity/Quality:

2,4-Dibromo-3,6-dimethoxyaniline 97% ^*data from reagent suppliers

Safty Information:

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Technology Process of 2,4-dibromo-3,6-dimethoxyaniline

There total 1 articles about 2,4-dibromo-3,6-dimethoxyaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,5-dimethoxyaniline (102-56-7,102526-87-4) → 2,4-dibromo-3,6-dimethoxyaniline (1160574-43-5)

Guidance literature:

With bromine; In dichloromethane; at -40 ℃; Inert atmosphere;

DOI:10.1021/ol300221e

Reference yield: 85.0%

2,4-dibromo-3,6-dimethoxyaniline (1160574-43-5) → 2,6-dibromo-1,4-dimethoxybenzene (74076-59-8)

Guidance literature:

With ethanol; sulfuric acid; sodium nitrite; In benzene; at 80 ℃; for 3h;

DOI:10.1021/jacs.7b01650

Reference yield: 73.0%

2,4-dibromo-3,6-dimethoxyaniline (1160574-43-5) + 1,1'-Thiocarbonyldiimidazole (6160-65-2) → 1,3-dibromo-4-isothiocyanato-2,5-dimethoxybenzene (1361383-45-0)

Guidance literature:

In 1,2-dichloro-ethane; at 60 ℃; for 50h; Inert atmosphere;

DOI:10.1021/ol300221e

upstream raw materials:

2,5-dimethoxyaniline

Downstream raw materials:

1,3-dibromo-4-isothiocyanato-2,5-dimethoxybenzene

2,6-dibromo-1,4-dimethoxybenzene

1,3-diiodo-2,5-dimethoxybenzene

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