Technology Process of C35H23N5
There total 6 articles about C35H23N5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
N,N-dimethyl-formamide;
at 90 ℃;
for 4h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / ethanol / 8 h / Inert atmosphere; Reflux
2: tetrabutylammomium bromide; acetic acid; potassium permanganate; water / dichloromethane / 5 h / Inert atmosphere
3: tin(II) chloride dihdyrate; hydrogenchloride / water; acetic acid / 1 h / Reflux
4: copper; 18-crown-6 ether; potassium carbonate / 1,2-dichloro-benzene / 4 h / Reflux; Inert atmosphere
5: potassium carbonate / N,N-dimethyl-formamide / 4 h / 90 °C / Inert atmosphere
With
hydrogenchloride; bis-triphenylphosphine-palladium(II) chloride; potassium permanganate; copper(l) iodide; 18-crown-6 ether; tin(II) chloride dihdyrate; tetrabutylammomium bromide; water; copper; potassium carbonate; acetic acid; triethylamine;
In
ethanol; dichloromethane; water; acetic acid; N,N-dimethyl-formamide; 1,2-dichloro-benzene;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: copper; 18-crown-6 ether; potassium carbonate / 1,2-dichloro-benzene / 4 h / Reflux; Inert atmosphere
2: potassium carbonate / N,N-dimethyl-formamide / 4 h / 90 °C / Inert atmosphere
With
18-crown-6 ether; copper; potassium carbonate;
In
N,N-dimethyl-formamide; 1,2-dichloro-benzene;