5,5,6,6,7,7-Hexamethyl-2,3-diphenyl-6,7-dihydro-5H-[2]pyrindinium; hydroxide

Base Information

• Chemical Name: 5,5,6,6,7,7-Hexamethyl-2,3-diphenyl-6,7-dihydro-5H-[2]pyrindinium; hydroxide
• CAS No.: 110373-08-5
• Molecular Formula: C₂₆H₃₀N*HO
• Molecular Weight: 373.538

Synonyms:5,5,6,6,7,7-Hexamethyl-2,3-diphenyl-6,7-dihydro-5H-[2]pyrindinium; hydroxide

Chemical Property of 5,5,6,6,7,7-Hexamethyl-2,3-diphenyl-6,7-dihydro-5H-[2]pyrindinium; hydroxide

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Technology Process of 5,5,6,6,7,7-Hexamethyl-2,3-diphenyl-6,7-dihydro-5H-[2]pyrindinium; hydroxide

There total 8 articles about 5,5,6,6,7,7-Hexamethyl-2,3-diphenyl-6,7-dihydro-5H-[2]pyrindinium; hydroxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

1,1,2,2,3,3-hexamethyl-4,5-bis(methylene)cyclopentane (96806-52-9) + C,N-diphenylnitrone (201024-81-9) → 5,5,6,6,7,7-Hexamethyl-3-phenyl-1,3,4,5,6,7-hexahydro-cyclopenta[d][1,2]oxazine (123186-98-1) + 6,6,7,7,8,8-Hexamethyl-3,4-diphenyl-3,4,5,6,7,8-hexahydro-1H-cyclopenta[e][1,2]oxazepine (110373-07-4) + 5,5,6,6,7,7-Hexamethyl-2,3-diphenyl-6,7-dihydro-5H-[2]pyrindinium; hydroxide (110373-08-5) + (S)-6,6,7,7,8,8-Hexamethyl-9-methylene-2,3-diphenyl-1-oxa-2-aza-spiro[4.4]nonane (123186-95-8)

Guidance literature:

In toluene; at 80 ℃; for 67h; Further byproducts given;

DOI:10.1021/jo00285a026

Reference yield: 28.0%

1,1,2,2,3,3-hexamethyl-4,5-bis(methylene)cyclopentane (96806-52-9) + C,N-diphenylnitrone (201024-81-9) → 6,6,7,7,8,8-Hexamethyl-3,4-diphenyl-3,4,5,6,7,8-hexahydro-1H-cyclopenta[e][1,2]oxazepine (110373-07-4) + 5,5,6,6,7,7-Hexamethyl-2,3-diphenyl-2,5,6,7-tetrahydro-[2]pyrindin-1-one (110373-09-6) + 5,5,6,6,7,7-Hexamethyl-2,3-diphenyl-6,7-dihydro-5H-[2]pyrindinium; hydroxide (110373-08-5) + (2R,3S,5S)-6,6,7,7,8,8-Hexamethyl-9-methylene-2,3-diphenyl-1-oxa-2-aza-spiro[4.4]nonane

Guidance literature:

In benzene; at 80 ℃; Further byproducts given;

DOI:10.1021/ja00255a052

Reference yield: 28.0%

1,1,2,2,3,3-hexamethyl-4,5-bis(methylene)cyclopentane (96806-52-9) + C,N-diphenylnitrone (201024-81-9) → 6,6,7,7,8,8-Hexamethyl-3,4-diphenyl-3,4,5,6,7,8-hexahydro-1H-cyclopenta[e][1,2]oxazepine (110373-07-4) + 5,5,6,6,7,7-Hexamethyl-2,3-diphenyl-6,7-dihydro-5H-[2]pyrindinium; hydroxide (110373-08-5) + (2S,3R,5S)-6,6,7,7,8,8-Hexamethyl-9-methylene-2,3-diphenyl-1-oxa-2-aza-spiro[4.4]nonane + (2R,3S,5S)-6,6,7,7,8,8-Hexamethyl-9-methylene-2,3-diphenyl-1-oxa-2-aza-spiro[4.4]nonane

Guidance literature:

In benzene; at 80 ℃; Further byproducts given;

DOI:10.1021/ja00255a052

upstream raw materials:

1,1,2,2,3,3-hexamethyl-4,5-bis(methylene)cyclopentane

C,N-diphenylnitrone

5,5,6,6,7,7-Hexamethyl-2,3-diphenyl-2,5,6,7-tetrahydro-[2]pyrindin-1-one

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