Technology Process of 4'-nitrophenyl 4-phenyl carbonate
There total 5 articles about 4'-nitrophenyl 4-phenyl carbonate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
triethylamine;
In
chloroform;
for 12h;
Ambient temperature;
DOI:10.1021/jm00026a013
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 30 percent / aq. AcOH / 48 h / Ambient temperature
2: 84 percent / KOH / ethanol / 2 h / Heating
3: 84 percent / CH3SO2Cl, pyridine / 0.25 h / 70 °C
4: 57 percent / H2, HCl / 30percent Pd/C / ethanol; diethyl ether
5: 67 percent / Et3N / CHCl3 / 12 h / Ambient temperature
With
pyridine; hydrogenchloride; potassium hydroxide; hydrogen; acetic acid; methanesulfonyl chloride; triethylamine;
palladium on activated charcoal;
In
diethyl ether; ethanol; chloroform;
DOI:10.1021/jm00026a013
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 84 percent / KOH / ethanol / 2 h / Heating
2: 84 percent / CH3SO2Cl, pyridine / 0.25 h / 70 °C
3: 57 percent / H2, HCl / 30percent Pd/C / ethanol; diethyl ether
4: 67 percent / Et3N / CHCl3 / 12 h / Ambient temperature
With
pyridine; hydrogenchloride; potassium hydroxide; hydrogen; methanesulfonyl chloride; triethylamine;
palladium on activated charcoal;
In
diethyl ether; ethanol; chloroform;
DOI:10.1021/jm00026a013