C₁₄H₁₈O₃

Base Information

Chemical Name:C₁₄H₁₈O₃
CAS No.:955030-25-8
Molecular Formula:C₁₄H₁₈O₃
Molecular Weight:234.295
Hs Code.:

C<sub>14</sub>H<sub>18</sub>O<sub>3</sub>

Synonyms:C₁₄H₁₈O₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₄H₁₈O₃

Chemical Property:

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Technology Process of C₁₄H₁₈O₃

There total 7 articles about C₁₄H₁₈O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 955030-40-7
C₁₄H₂₀O₃

: 955030-25-8
C₁₄H₁₈O₃

Guidance literature:: With 2,2,6,6-tetramethyl-piperidine-N-oxyl; In dichloromethane;
DOI:10.1016/j.tetlet.2007.07.156

Reference yield:

: 955030-24-7
C₁₄H₁₈O₃

: 955030-25-8
C₁₄H₁₈O₃

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / DIBAL-H / CH₂Cl₂ / 0 °C

2: 95 percent / TEMPO; IBDA / CH₂Cl₂

With 2,2,6,6-tetramethyl-piperidine-N-oxyl; diisobutylaluminium hydride; In dichloromethane;
DOI:10.1016/j.tetlet.2007.07.156

Reference yield:

: C₁₂H₂₆O₂Si

: 955030-25-8
C₁₄H₁₈O₃

Guidance literature:: Multi-step reaction with 6 steps

1: titanium(IV) isopropylate; Cumene hydroperoxide; D-(-)-diisopropyl tartrate / dichloromethane / -20 °C

2: 1H-imidazole; iodine; triphenylphosphine / tetrahydrofuran / 0.5 h

3: ethanol; zinc / 3 h / 80 °C

4: sodium hydride / tetrahydrofuran / 14 h / 0 - 20 °C

5: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h

6: oxalyl dichloride; dimethyl sulfoxide; triethylamine / 1 h / -78 °C

With 1H-imidazole; titanium(IV) isopropylate; oxalyl dichloride; ethanol; Cumene hydroperoxide; tetrabutyl ammonium fluoride; iodine; sodium hydride; D-(-)-diisopropyl tartrate; dimethyl sulfoxide; triethylamine; triphenylphosphine; zinc; In tetrahydrofuran; dichloromethane; 1: Sharpless asymmetric epoxidation / 6: Swern oxidation;
DOI:10.1016/j.tetlet.2011.06.087