C₂₅H₃₂O₄Si

Base Information Edit

Chemical Name:C₂₅H₃₂O₄Si
CAS No.:1440510-01-9
Molecular Formula:C₂₅H₃₂O₄Si
Molecular Weight:424.612
Hs Code.:
Mol file:1440510-01-9.mol

C<sub>25</sub>H<sub>32</sub>O<sub>4</sub>Si

Synonyms:C₂₅H₃₂O₄Si

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Chemical Property of C₂₅H₃₂O₄Si Edit

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Technology Process of C₂₅H₃₂O₄Si

There total 7 articles about C₂₅H₃₂O₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 902799-70-6
C₂₇H₃₆SiO₄

: 1440510-01-9
C₂₅H₃₂O₄Si

Guidance literature:: With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; Reflux;
DOI:10.1039/c3md00021d

Reference yield:

: 67814-68-0,70266-87-4,76249-50-8,76249-51-9,93451-15-1,4099-88-1
2,3-O-isopropylidene-D-ribofuranose

: 1440510-01-9
C₂₅H₃₂O₄Si

Guidance literature:: Multi-step reaction with 5 steps

1: triethylamine; dmap / N,N-dimethyl-formamide

2: potassium tert-butylate / tetrahydrofuran

3: triethylamine; sulfur trioxide pyridine complex / dichloromethane

4: tetrahydrofuran / -78 °C

5: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / Reflux

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; dmap; potassium tert-butylate; sulfur trioxide pyridine complex; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 2: |Wittig Olefination;
DOI:10.1039/c3md00021d

Reference yield:

: 96690-02-7
5-O-(tert-butyldiphenylsilyl)-2,3-O-isopropylidene-D-ribofuranose

: 1440510-01-9
C₂₅H₃₂O₄Si

Guidance literature:: Multi-step reaction with 4 steps

1: potassium tert-butylate / tetrahydrofuran

2: triethylamine; sulfur trioxide pyridine complex / dichloromethane

3: tetrahydrofuran / -78 °C

4: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / Reflux

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; potassium tert-butylate; sulfur trioxide pyridine complex; triethylamine; In tetrahydrofuran; dichloromethane; 1: |Wittig Olefination;
DOI:10.1039/c3md00021d