P,P-diphenyl-N-{1-[dimethyl(phenyl)silyl]-1-phenylethyl}phosphinic amide

Base Information

Chemical Name:P,P-diphenyl-N-{1-[dimethyl(phenyl)silyl]-1-phenylethyl}phosphinic amide
CAS No.:1283154-38-0
Molecular Formula:C₂₉H₃₂NOPSi
Molecular Weight:469.638
Hs Code.:

Synonyms:P,P-diphenyl-N-{1-[dimethyl(phenyl)silyl]-1-phenylethyl}phosphinic amide

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Chemical Property of P,P-diphenyl-N-{1-[dimethyl(phenyl)silyl]-1-phenylethyl}phosphinic amide

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Technology Process of P,P-diphenyl-N-{1-[dimethyl(phenyl)silyl]-1-phenylethyl}phosphinic amide

There total 3 articles about P,P-diphenyl-N-{1-[dimethyl(phenyl)silyl]-1-phenylethyl}phosphinic amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 185990-03-8
dimethylphenyl(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)silane

: 942066-05-9
N-[(1E)-1-phenylpropylidene]-P,P-diphenylphosphinic amide

: 1283154-38-0
P,P-diphenyl-N-{1-[dimethyl(phenyl)silyl]-1-phenylethyl}phosphinic amide

Guidance literature:: With methanol; sodium methylate; copper(l) cyanide; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol200509c

Reference yield:

: 2157-50-8
propiophenone oxime

: 1283154-38-0
P,P-diphenyl-N-{1-[dimethyl(phenyl)silyl]-1-phenylethyl}phosphinic amide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / hexane; dichloromethane / -40 - 20 °C / Inert atmosphere

2: methanol; sodium methylate; copper(l) cyanide / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

With methanol; sodium methylate; copper(l) cyanide; triethylamine; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1021/ol200509c

Reference yield:

: 93-55-0
1-phenyl-propan-1-one

: 1283154-38-0
P,P-diphenyl-N-{1-[dimethyl(phenyl)silyl]-1-phenylethyl}phosphinic amide

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen chloride - ammonia - water; sodium acetate / methanol / 12.5 h / 20 °C / Inert atmosphere

2: triethylamine / hexane; dichloromethane / -40 - 20 °C / Inert atmosphere

3: methanol; sodium methylate; copper(l) cyanide / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

With methanol; hydrogen chloride - ammonia - water; sodium methylate; sodium acetate; copper(l) cyanide; triethylamine; In tetrahydrofuran; methanol; hexane; dichloromethane;
DOI:10.1021/ol200509c