2-(2′,6′-dimethylphenyl)imidazo[1,5-a]pyridin-2-ium hexafluorophosphate

Base Information

Chemical Name:2-(2′,6′-dimethylphenyl)imidazo[1,5-a]pyridin-2-ium hexafluorophosphate
CAS No.:1610846-64-4
Molecular Formula:C₁₅H₁₅N₂*F₆P
Molecular Weight:368.262
Hs Code.:

Synonyms:2-(2′,6′-dimethylphenyl)imidazo[1,5-a]pyridin-2-ium hexafluorophosphate

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Chemical Property of 2-(2′,6′-dimethylphenyl)imidazo[1,5-a]pyridin-2-ium hexafluorophosphate

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Technology Process of 2-(2′,6′-dimethylphenyl)imidazo[1,5-a]pyridin-2-ium hexafluorophosphate

There total 3 articles about 2-(2′,6′-dimethylphenyl)imidazo[1,5-a]pyridin-2-ium hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.6%

: 110-88-3
1,3,5-Trioxan

: 29167-92-8,1610846-62-2
2,6-dimethylphenyl-N-(pyridin-2-ylmethyl)benzeneamine

: 1610846-64-4
2-(2′,6′-dimethylphenyl)imidazo[1,5-a]pyridin-2-ium hexafluorophosphate

Guidance literature:: 1,3,5-Trioxan; 2,6-dimethylphenyl-N-(pyridin-2-ylmethyl)benzeneamine; With hydrogenchloride; In 1,4-dioxane; toluene; at 20 ℃; for 15h; Schlenk technique; Inert atmosphere;

With potassium hexafluorophosphate; In water; Schlenk technique; Inert atmosphere;
DOI:10.1039/c4dt00695j

Reference yield:

: 87-62-7
2,6-dimethylaniline

: 1610846-64-4
2-(2′,6′-dimethylphenyl)imidazo[1,5-a]pyridin-2-ium hexafluorophosphate

Guidance literature:: Multi-step reaction with 2 steps

1.1: molecular sieve (4 ?) / toluene / Schlenk technique; Inert atmosphere

2.1: hydrogenchloride / toluene; 1,4-dioxane / 15 h / 20 °C / Schlenk technique; Inert atmosphere

2.2: Schlenk technique; Inert atmosphere

With hydrogenchloride; In 1,4-dioxane; toluene;
DOI:10.1039/c4dt00695j

Reference yield:

: 1121-60-4
pyridine-2-carbaldehyde

: 1610846-64-4
2-(2′,6′-dimethylphenyl)imidazo[1,5-a]pyridin-2-ium hexafluorophosphate

Guidance literature:: Multi-step reaction with 2 steps

1.1: molecular sieve (4 ?) / toluene / Schlenk technique; Inert atmosphere

2.1: hydrogenchloride / toluene; 1,4-dioxane / 15 h / 20 °C / Schlenk technique; Inert atmosphere

2.2: Schlenk technique; Inert atmosphere

With hydrogenchloride; In 1,4-dioxane; toluene;
DOI:10.1039/c4dt00695j