3-(t-butyldimethylsilyloxy)-7-hexyl-2-phenylsulphonyltetrahydro-4,5,6,7-oxepine

Base Information

Chemical Name:3-(t-butyldimethylsilyloxy)-7-hexyl-2-phenylsulphonyltetrahydro-4,5,6,7-oxepine
CAS No.:132834-84-5
Molecular Formula:C₂₄H₄₀O₄SSi
Molecular Weight:452.731
Hs Code.:

Synonyms:3-(t-butyldimethylsilyloxy)-7-hexyl-2-phenylsulphonyltetrahydro-4,5,6,7-oxepine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(t-butyldimethylsilyloxy)-7-hexyl-2-phenylsulphonyltetrahydro-4,5,6,7-oxepine

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Technology Process of 3-(t-butyldimethylsilyloxy)-7-hexyl-2-phenylsulphonyltetrahydro-4,5,6,7-oxepine

There total 1 articles about 3-(t-butyldimethylsilyloxy)-7-hexyl-2-phenylsulphonyltetrahydro-4,5,6,7-oxepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 69739-34-0
t-butyldimethylsiyl triflate

: 128699-21-8,132834-82-3
7-hexyl-2-phenylsulphonyloxepan-3-one

: 132834-84-5
3-(t-butyldimethylsilyloxy)-7-hexyl-2-phenylsulphonyltetrahydro-4,5,6,7-oxepine

Guidance literature:: With triethylamine; In dichloromethane; for 5h; Ambient temperature;

Reference yield:

: 132834-84-5
3-(t-butyldimethylsilyloxy)-7-hexyl-2-phenylsulphonyltetrahydro-4,5,6,7-oxepine

: 132834-86-7
7-hexyl-2-propyloxepan-3-one tosylhydrazone

Guidance literature:: Multi-step reaction with 3 steps

1: 1) tetrabutylammonium fluoride / 1) THF, -78 deg C, 15 min, 2) up to room temperature, overnight

2: tributyltin hydride, AIBN / toluene

3: 82 percent / toluene 4-sulphonic acid, 4 Angstroem sieves / methanol / 36 h

With 2,2'-azobis(isobutyronitrile); 4 A molecular sieve; tetrabutyl ammonium fluoride; tri-n-butyl-tin hydride; toluene-4-sulfonic acid; In methanol; toluene;

Reference yield:

: 132834-84-5
3-(t-butyldimethylsilyloxy)-7-hexyl-2-phenylsulphonyltetrahydro-4,5,6,7-oxepine

: 107-08-4
1-iodo-propane

: 132834-85-6
7-hexyl-2-phenylsulphonyl-2-propyloxepan-3-one

Guidance literature:: With tetrabutyl ammonium fluoride; Yield given. Multistep reaction; 1) THF, -78 deg C, 15 min, 2) up to room temperature, overnight;