[2-methyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]methyl methyl carbonate

Base Information

Chemical Name:[2-methyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]methyl methyl carbonate
CAS No.:1350906-77-2
Molecular Formula:C₁₆H₂₃BO₅
Molecular Weight:306.167
Hs Code.:

Synonyms:[2-methyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]methyl methyl carbonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [2-methyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]methyl methyl carbonate

Chemical Property:

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Technology Process of [2-methyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]methyl methyl carbonate

There total 3 articles about [2-methyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]methyl methyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1350906-74-9
(3-bromo-2-methylphenyl)methyl methyl carbonate

: 73183-34-3
bis(pinacol)diborane

: 1350906-77-2
[2-methyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]methyl methyl carbonate

Guidance literature:: With potassium acetate; palladium diacetate; triphenylphosphine; In N,N-dimethyl-formamide; at 80 ℃; for 24h;
DOI:10.1021/ol203089k

Reference yield:

: 258886-04-3
(5-bromo-2-methylphenyl)methanol

: 1350906-77-2
[2-methyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]methyl methyl carbonate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; dmap / dichloromethane / 0 - 20 °C / Inert atmosphere

2: potassium acetate; palladium diacetate; triphenylphosphine / N,N-dimethyl-formamide / 24 h / 80 °C

With pyridine; dmap; potassium acetate; palladium diacetate; triphenylphosphine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol203089k

Reference yield:

: 79669-49-1
5-bromo-2-methylbenzoic acid

: 1350906-77-2
[2-methyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]methyl methyl carbonate

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Reflux; Inert atmosphere

2: pyridine; dmap / dichloromethane / 0 - 20 °C / Inert atmosphere

3: potassium acetate; palladium diacetate; triphenylphosphine / N,N-dimethyl-formamide / 24 h / 80 °C

With pyridine; dmap; lithium aluminium tetrahydride; potassium acetate; palladium diacetate; triphenylphosphine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol203089k