13-cyano-9,12-di(phenylmethyl)-2,2-dimethyl-3-oxa-4-oxo-5,9,12-triazotridecane

Base Information

Chemical Name:13-cyano-9,12-di(phenylmethyl)-2,2-dimethyl-3-oxa-4-oxo-5,9,12-triazotridecane
CAS No.:154920-42-0
Molecular Formula:C₂₆H₃₆N₄O₂
Molecular Weight:436.597
Hs Code.:

Synonyms:13-cyano-9,12-di(phenylmethyl)-2,2-dimethyl-3-oxa-4-oxo-5,9,12-triazotridecane

Suppliers and Price of 13-cyano-9,12-di(phenylmethyl)-2,2-dimethyl-3-oxa-4-oxo-5,9,12-triazotridecane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 13-cyano-9,12-di(phenylmethyl)-2,2-dimethyl-3-oxa-4-oxo-5,9,12-triazotridecane

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 13-cyano-9,12-di(phenylmethyl)-2,2-dimethyl-3-oxa-4-oxo-5,9,12-triazotridecane

There total 10 articles about 13-cyano-9,12-di(phenylmethyl)-2,2-dimethyl-3-oxa-4-oxo-5,9,12-triazotridecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 107-14-2
chloroacetonitrile

: 154920-41-9
9,12-di(phenylmethyl)-2,2-dimethyl-3-oxa-4-oxo-5,9,12-triazododecane

: 154920-42-0
13-cyano-9,12-di(phenylmethyl)-2,2-dimethyl-3-oxa-4-oxo-5,9,12-triazotridecane

Guidance literature:: With potassium fluoride; Celite; In acetonitrile; at 85 ℃; for 12h;
DOI:10.1002/jhet.5570300532

Reference yield:

: 58632-95-4
2-(tert-Butoxycarbonyloxyimino)-2-phenylacetonitrile

: 154920-42-0
13-cyano-9,12-di(phenylmethyl)-2,2-dimethyl-3-oxa-4-oxo-5,9,12-triazotridecane

Guidance literature:: Multi-step reaction with 6 steps

1: 81 percent / tetrahydrofuran / 6 h / Ambient temperature

2: 87 percent / potassium fluoride/celite / acetonitrile / 12 h / 85 °C

3: 92 percent / H₂, aq. NaOH / Raney Ni / ethanol / 12 h / 2327.2 Torr

4: magnesium sulfate / methanol / 4 h / Ambient temperature

5: NaBH₄ / methanol / Ambient temperature

6: 96 percent / KF/celite / acetonitrile / 12 h / 85 °C

With potassium fluoride; sodium hydroxide; sodium tetrahydroborate; Celite; hydrogen; magnesium sulfate; nickel; In tetrahydrofuran; methanol; ethanol; acetonitrile;
DOI:10.1002/jhet.5570300532

Reference yield:

: 90914-08-2
N-[N-(tert-Butyloxycarbonyl)-3-aminopropyl]benzylamine

: 154920-42-0
13-cyano-9,12-di(phenylmethyl)-2,2-dimethyl-3-oxa-4-oxo-5,9,12-triazotridecane

Guidance literature:: Multi-step reaction with 5 steps

1: 87 percent / potassium fluoride/celite / acetonitrile / 12 h / 85 °C

2: 92 percent / H₂, aq. NaOH / Raney Ni / ethanol / 12 h / 2327.2 Torr

3: magnesium sulfate / methanol / 4 h / Ambient temperature

4: NaBH₄ / methanol / Ambient temperature

5: 96 percent / KF/celite / acetonitrile / 12 h / 85 °C

With potassium fluoride; sodium hydroxide; sodium tetrahydroborate; Celite; hydrogen; magnesium sulfate; nickel; In methanol; ethanol; acetonitrile;
DOI:10.1002/jhet.5570300532