1-Benzyloxymethyl-3-[1-((3aR,4S,6R,7aR)-1-benzyloxymethyl-4-hydroxymethyl-2-oxo-hexahydro-pyrano[4,3-d]oxazol-6-yl)-1H-indol-3-yl]-4-(1H-indol-3-yl)-pyrrole-2,5-dione

Base Information

• Chemical Name: 1-Benzyloxymethyl-3-[1-((3aR,4S,6R,7aR)-1-benzyloxymethyl-4-hydroxymethyl-2-oxo-hexahydro-pyrano[4,3-d]oxazol-6-yl)-1H-indol-3-yl]-4-(1H-indol-3-yl)-pyrrole-2,5-dione
• CAS No.: 160256-44-0
• Molecular Formula: C₄₃H₃₈N₄O₈
• Molecular Weight: 738.797

Synonyms:1-Benzyloxymethyl-3-[1-((3aR,4S,6R,7aR)-1-benzyloxymethyl-4-hydroxymethyl-2-oxo-hexahydro-pyrano[4,3-d]oxazol-6-yl)-1H-indol-3-yl]-4-(1H-indol-3-yl)-pyrrole-2,5-dione

Chemical Property of 1-Benzyloxymethyl-3-[1-((3aR,4S,6R,7aR)-1-benzyloxymethyl-4-hydroxymethyl-2-oxo-hexahydro-pyrano[4,3-d]oxazol-6-yl)-1H-indol-3-yl]-4-(1H-indol-3-yl)-pyrrole-2,5-dione

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Technology Process of 1-Benzyloxymethyl-3-[1-((3aR,4S,6R,7aR)-1-benzyloxymethyl-4-hydroxymethyl-2-oxo-hexahydro-pyrano[4,3-d]oxazol-6-yl)-1H-indol-3-yl]-4-(1H-indol-3-yl)-pyrrole-2,5-dione

There total 1 articles about 1-Benzyloxymethyl-3-[1-((3aR,4S,6R,7aR)-1-benzyloxymethyl-4-hydroxymethyl-2-oxo-hexahydro-pyrano[4,3-d]oxazol-6-yl)-1H-indol-3-yl]-4-(1H-indol-3-yl)-pyrrole-2,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

1-Benzyloxymethyl-3-[1-((3aR,4S,6R,7aR)-1-benzyloxymethyl-4-hydroxymethyl-2-oxo-hexahydro-pyrano[4,3-d]oxazol-6-yl)-1H-indol-3-yl]-4-[1-(2-trimethylsilanyl-ethoxymethyl)-1H-indol-3-yl]-pyrrole-2,5-dione → 1-Benzyloxymethyl-3-[1-((3aR,4S,6R,7aR)-1-benzyloxymethyl-4-hydroxymethyl-2-oxo-hexahydro-pyrano[4,3-d]oxazol-6-yl)-1H-indol-3-yl]-4-(1H-indol-3-yl)-pyrrole-2,5-dione (160256-44-0)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; Heating;

DOI:10.1021/ja00106a072

Reference yield: 88.0%

1-Benzyloxymethyl-3-[1-((3aR,4S,6R,7aR)-1-benzyloxymethyl-4-hydroxymethyl-2-oxo-hexahydro-pyrano[4,3-d]oxazol-6-yl)-1H-indol-3-yl]-4-(1H-indol-3-yl)-pyrrole-2,5-dione (160256-44-0) → 1-Benzyloxymethyl-3-[1-((3aR,4R,6R,7aR)-1-benzyloxymethyl-4-iodomethyl-2-oxo-hexahydro-pyrano[4,3-d]oxazol-6-yl)-1H-indol-3-yl]-4-(1H-indol-3-yl)-pyrrole-2,5-dione (174148-64-2)

Guidance literature:

With 1H-imidazole; iodine; triphenylphosphine; at 0 - 20 ℃;

DOI:10.1021/ja952907g

Reference yield: 73.0%

1-Benzyloxymethyl-3-[1-((3aR,4S,6R,7aR)-1-benzyloxymethyl-4-hydroxymethyl-2-oxo-hexahydro-pyrano[4,3-d]oxazol-6-yl)-1H-indol-3-yl]-4-(1H-indol-3-yl)-pyrrole-2,5-dione (160256-44-0) → C43H36N4O8

Guidance literature:

With iodine; In benzene; Ambient temperature; Irradiation;

DOI:10.1021/ja00106a072

Downstream raw materials:

1-Benzyloxymethyl-3-[1-((3aR,4R,6R,7aR)-1-benzyloxymethyl-4-iodomethyl-2-oxo-hexahydro-pyrano[4,3-d]oxazol-6-yl)-1H-indol-3-yl]-4-(1H-indol-3-yl)-pyrrole-2,5-dione

C₄₃H₃₆N₄O₆

3-{1-Benzyloxymethyl-4-[1-((3aR,6R,7aR)-1-benzyloxymethyl-4-methylene-2-oxo-hexahydro-pyrano[4,3-d]oxazol-6-yl)-1H-indol-3-yl]-2,5-dioxo-2,5-dihydro-1H-pyrrol-3-yl}-indole-1-carboxylic acid benzyl ester

3-{1-Benzyloxymethyl-4-[1-((3aR,4R,6R,7aR)-1-benzyloxymethyl-4-iodomethyl-2-oxo-hexahydro-pyrano[4,3-d]oxazol-6-yl)-1H-indol-3-yl]-2,5-dioxo-2,5-dihydro-1H-pyrrol-3-yl}-indole-1-carboxylic acid benzyl ester

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