methyl β-(2,3,4,6-tetra-O-acetyl-D-glucopyranosyl-(1->4)-β-(2,3,6-tri-O-acetyl-D-glucopyranosyl)-(1->4)-β-2,3,6-tri-O-benzoyl)-4-thio-D-glucoside

Base Information

Chemical Name:methyl β-(2,3,4,6-tetra-O-acetyl-D-glucopyranosyl-(1->4)-β-(2,3,6-tri-O-acetyl-D-glucopyranosyl)-(1->4)-β-2,3,6-tri-O-benzoyl)-4-thio-D-glucoside
CAS No.:1315206-25-7
Molecular Formula:C₅₄H₆₀O₂₅S
Molecular Weight:1141.12
Hs Code.:

Synonyms:methyl β-(2,3,4,6-tetra-O-acetyl-D-glucopyranosyl-(1->4)-β-(2,3,6-tri-O-acetyl-D-glucopyranosyl)-(1->4)-β-2,3,6-tri-O-benzoyl)-4-thio-D-glucoside

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Chemical Property of methyl β-(2,3,4,6-tetra-O-acetyl-D-glucopyranosyl-(1->4)-β-(2,3,6-tri-O-acetyl-D-glucopyranosyl)-(1->4)-β-2,3,6-tri-O-benzoyl)-4-thio-D-glucoside

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Technology Process of methyl β-(2,3,4,6-tetra-O-acetyl-D-glucopyranosyl-(1->4)-β-(2,3,6-tri-O-acetyl-D-glucopyranosyl)-(1->4)-β-2,3,6-tri-O-benzoyl)-4-thio-D-glucoside

There total 3 articles about methyl β-(2,3,4,6-tetra-O-acetyl-D-glucopyranosyl-(1->4)-β-(2,3,6-tri-O-acetyl-D-glucopyranosyl)-(1->4)-β-2,3,6-tri-O-benzoyl)-4-thio-D-glucoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 68636-40-8
2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl-(1→4)-2,3,6-tri-O-acetyl-1-thio-β-D-glucopyranose

: 124314-27-8
methyl 2,3,6-tri-O-benzoyl-4-O-(trifluoromethylsulfonyl)-β-D-galactopyranoside

: 1315206-25-7
methyl β-(2,3,4,6-tetra-O-acetyl-D-glucopyranosyl-(1->4)-β-(2,3,6-tri-O-acetyl-D-glucopyranosyl)-(1->4)-β-2,3,6-tri-O-benzoyl)-4-thio-D-glucoside

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 0 ℃; for 1h; Inert atmosphere;
DOI:10.1016/j.bmc.2011.04.048

Reference yield:

: 6344-46-3
methyl 2,3,6-tri-O-benzoyl β-D-galactopyranoside

: 1315206-25-7
methyl β-(2,3,4,6-tetra-O-acetyl-D-glucopyranosyl-(1->4)-β-(2,3,6-tri-O-acetyl-D-glucopyranosyl)-(1->4)-β-2,3,6-tri-O-benzoyl)-4-thio-D-glucoside

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 0.33 h / 0 °C / Inert atmosphere

2: sodium hydride / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

With pyridine; sodium hydride; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.bmc.2011.04.048

Reference yield:

: 205451-24-7
2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl-(1→4)-2,3,6-tri-O-acetyl-1-S-acetyl-1-thio-β-D-glucopyranose

: 1315206-25-7
methyl β-(2,3,4,6-tetra-O-acetyl-D-glucopyranosyl-(1->4)-β-(2,3,6-tri-O-acetyl-D-glucopyranosyl)-(1->4)-β-2,3,6-tri-O-benzoyl)-4-thio-D-glucoside

Guidance literature:: Multi-step reaction with 2 steps

1: sodium methylate / methanol; dichloromethane / 0.5 h / -15 °C / Inert atmosphere

2: sodium hydride / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

With sodium methylate; sodium hydride; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/j.bmc.2011.04.048