1,3-Diphenyl-8-methyldibenzo-8-thiaazulene

Base Information

• Chemical Name: 1,3-Diphenyl-8-methyldibenzo-8-thiaazulene
• CAS No.: 77189-49-2
• Molecular Formula: C₃₀H₂₂S
• Molecular Weight: 414.571

Synonyms:1,3-Diphenyl-8-methyldibenzo-8-thiaazulene

Chemical Property of 1,3-Diphenyl-8-methyldibenzo-8-thiaazulene

Chemical Property:

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Technology Process of 1,3-Diphenyl-8-methyldibenzo-8-thiaazulene

There total 1 articles about 1,3-Diphenyl-8-methyldibenzo-8-thiaazulene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

8-Methyl-1,3-diphenyl-2H-8-thionia-dibenzo[e,h]azulene; perchlorate → 1,3-Diphenyl-8-methyldibenzo-8-thiaazulene (77189-49-2)

Guidance literature:

With sodium hydride; In tetrahydrofuran; Ambient temperature;

DOI:10.1016/S0040-4039(00)92885-5

Reference yield: 71.0%

1,3-Diphenyl-8-methyldibenzo-8-thiaazulene (77189-49-2) + dimethyl acetylenedicarboxylate (762-42-5) → C36H27(2)HO4S

Guidance literature:

With water-d2;

Reference yield: 70.0%

1,3-Diphenyl-8-methyldibenzo-8-thiaazulene (77189-49-2) + acetylenedicarboxylic acid diethyl ester (762-21-0) → (E)-2-(8-Methyl-1,3-diphenyl-8λ4-thia-dibenzo[e,h]azulen-2-yl)-but-2-enedioic acid diethyl ester (78311-43-0)

Guidance literature:

Downstream raw materials:

1,3-Diphenyl-2,8-dihydrodibenzo-8-thiaazulene

1,3-diphenyl-12b-methyl-8,12b-dihydrodibenzo-8-thiaazulene

(E)-2-(8-Methyl-1,3-diphenyl-8λ⁴-thia-dibenzo[e,h]azulen-2-yl)-but-2-enedioic acid dimethyl ester

(Z)-2-(8-Methyl-1,3-diphenyl-8λ⁴-thia-dibenzo[e,h]azulen-2-yl)-but-2-enedioic acid dimethyl ester

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