5-butyl-2-hydroxymethyl-1-<<2'-<(N-triphenylmethyl)tetrazol-5-yl>biphenyl-4-yl>methyl>imidazole

Base Information

Chemical Name:5-butyl-2-hydroxymethyl-1-<<2'-<(N-triphenylmethyl)tetrazol-5-yl>biphenyl-4-yl>methyl>imidazole
CAS No.:155091-95-5
Molecular Formula:C₄₁H₃₈N₆O
Molecular Weight:630.792
Hs Code.:

Synonyms:5-butyl-2-hydroxymethyl-1-<<2'-<(N-triphenylmethyl)tetrazol-5-yl>biphenyl-4-yl>methyl>imidazole

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Chemical Property of 5-butyl-2-hydroxymethyl-1-<<2'-<(N-triphenylmethyl)tetrazol-5-yl>biphenyl-4-yl>methyl>imidazole

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Technology Process of 5-butyl-2-hydroxymethyl-1-<<2'-<(N-triphenylmethyl)tetrazol-5-yl>biphenyl-4-yl>methyl>imidazole

There total 19 articles about 5-butyl-2-hydroxymethyl-1-<<2'-<(N-triphenylmethyl)tetrazol-5-yl>biphenyl-4-yl>methyl>imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1400933-88-1
5-butyl-2-hydroxymethyl-1-[[(2'-(2-trityl)-2H-tetrazol-5-yl)biphenyl-4-yl]methyl]-3-[(2-(trimethylsilyl)ethoxy)methyl]-1H-imidazolium bromide

: 155091-95-5
5-butyl-2-hydroxymethyl-1-<<2'-<(N-triphenylmethyl)tetrazol-5-yl>biphenyl-4-yl>methyl>imidazole

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; for 8h; Inert atmosphere; Reflux;
DOI:10.1016/j.ejmech.2012.07.040

Reference yield: 66.0%

: 155091-94-4
1-<<2'-<(N-triphenylmethyl)tetrazol-5-yl>biphenyl-4-yl>methyl>-5-butylimidazole-2-carboxaldehyde

: 155091-95-5
5-butyl-2-hydroxymethyl-1-<<2'-<(N-triphenylmethyl)tetrazol-5-yl>biphenyl-4-yl>methyl>imidazole

Guidance literature:: With sodium tetrahydroborate; In methanol; N,N-dimethyl-formamide; for 1.5h; Ambient temperature;

Reference yield:

: 146953-86-8
4-n-Butyl-imidazole

: 155091-95-5
5-butyl-2-hydroxymethyl-1-<<2'-<(N-triphenylmethyl)tetrazol-5-yl>biphenyl-4-yl>methyl>imidazole

Guidance literature:: Multi-step reaction with 7 steps

1: 84 percent / Et₃N / acetonitrile / 1 h / Ambient temperature

2: 38 percent / acetonitrile / 1.) reflux, 4 h; 2.) RT

3: 37 percent / H₂O / 6 h / 140 °C / Curtius tube

4: 98 percent / Na/NH₃(l) / methanol / 0.08 h

5: 85 percent / MnO₂ / CH₂Cl₂ / Ambient temperature

6: cesium carbonate / dimethylformamide / Ambient temperature

7: 66 percent / NaBH₄ / methanol; dimethylformamide / 1.5 h / Ambient temperature

With manganese(IV) oxide; sodium tetrahydroborate; ammonia; sodium; caesium carbonate; triethylamine; In methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;