dimesitylvinylfluorosilane

Base Information

• Chemical Name: dimesitylvinylfluorosilane
• CAS No.: 160011-52-9
• Molecular Formula: C₂₀H₂₅FSi
• Molecular Weight: 312.502
• Mol file: 160011-52-9.mol

Synonyms:dimesitylvinylfluorosilane

Chemical Property of dimesitylvinylfluorosilane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of dimesitylvinylfluorosilane

There total 3 articles about dimesitylvinylfluorosilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

dimesitylfluorosilane (119106-07-9) + acetylene (74-86-2,25067-58-7) → dimesitylvinylfluorosilane (160011-52-9)

Guidance literature:

With dihydrogen hexachloroplatinate; In tetrahydrofuran; benzene; at 75 ℃; for 18h;

DOI:10.1016/0022-328X(95)06036-V

Reference yield:

2,4,6-trimethylphenyl bromide (576-83-0) → dimesitylvinylfluorosilane (160011-52-9)

Guidance literature:

Multi-step reaction with 3 steps

1: 1.) magnesium, 2.) trichlorosilane / 1.) THF, 2.) ether, THF, 0 deg C; reflux, 1 h 30 min

2: 67 percent / 40percent aq. HF

3: 97 percent / H₂PtCl₆ / benzene; tetrahydrofuran / 18 h / 75 °C

With dihydrogen hexachloroplatinate; trichlorosilane; hydrogen fluoride; magnesium; In tetrahydrofuran; benzene;

DOI:10.1016/0022-328X(95)06036-V

Reference yield:

chloro-di-(2,4,6-trimethylphenyl)silane (50490-74-9) → dimesitylvinylfluorosilane (160011-52-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 67 percent / 40percent aq. HF

2: 97 percent / H₂PtCl₆ / benzene; tetrahydrofuran / 18 h / 75 °C

With dihydrogen hexachloroplatinate; hydrogen fluoride; In tetrahydrofuran; benzene;

DOI:10.1016/0022-328X(95)06036-V

upstream raw materials:

dimesitylfluorosilane

acetylene

2,4,6-trimethylphenyl bromide

chloro-di-(2,4,6-trimethylphenyl)silane

Downstream raw materials:

1,1-dimesitylneopentylsilene

bis(mesityl)silanediol

tert-Butyl-[1-tert-butyl-4-[3,3-dimethyl-but-(E)-ylidene]-3,3-bis-(2,4,6-trimethyl-phenyl)-[1,3]azasiletidin-(2E)-ylidene]-amine