pentafluoro-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-6-sulfane

Base Information

Chemical Name:pentafluoro-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-6-sulfane
CAS No.:1286278-34-9
Molecular Formula:C₁₂H₁₆BF₅O₂S
Molecular Weight:330.127
Hs Code.:

Synonyms:pentafluoro-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-6-sulfane

Suppliers and Price of pentafluoro-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-6-sulfane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 4 raw suppliers

Chemical Property of pentafluoro-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-6-sulfane

Chemical Property:

Purity/Quality:: 97% ^*data from raw suppliers

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Technology Process of pentafluoro-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-6-sulfane

There total 9 articles about pentafluoro-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-6-sulfane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 774-93-6
1-bromo-4-pentafluorosulfanylbenzene

: 73183-34-3
bis(pinacol)diborane

: 1286278-34-9
pentafluoro-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-6-sulfane

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; In 1,4-dioxane; at 100 ℃; for 16h;

Reference yield: 78.0%

: tetrafluoroboric acid

: 2993-24-0
4-(pentafluorosulfanyl)aniline

: 73183-34-3
bis(pinacol)diborane

: 1286278-34-9
pentafluoro-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-6-sulfane

Guidance literature:: tetrafluoroboric acid; 4-(pentafluorosulfanyl)aniline; With tert.-butylnitrite; In acetonitrile; at 0 ℃; for 0.333333h;

bis(pinacol)diborane; With pyridine; In acetonitrile; at -25 - 25 ℃; for 1h;
DOI:10.3762/bjoc.11.162