2,3,4-tri-O-benzoyl-α-D-glucopyranosyl tetramethylphosphoroamidate

Base Information

Chemical Name:2,3,4-tri-O-benzoyl-α-D-glucopyranosyl tetramethylphosphoroamidate
CAS No.:193953-61-6
Molecular Formula:C₃₁H₃₅N₂O₁₀P
Molecular Weight:626.6
Hs Code.:

Synonyms:2,3,4-tri-O-benzoyl-α-D-glucopyranosyl tetramethylphosphoroamidate

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Chemical Property of 2,3,4-tri-O-benzoyl-α-D-glucopyranosyl tetramethylphosphoroamidate

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Technology Process of 2,3,4-tri-O-benzoyl-α-D-glucopyranosyl tetramethylphosphoroamidate

There total 7 articles about 2,3,4-tri-O-benzoyl-α-D-glucopyranosyl tetramethylphosphoroamidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 143520-19-8
C₃₈H₄₇N₂O₇P

: 193953-61-6
2,3,4-tri-O-benzoyl-α-D-glucopyranosyl tetramethylphosphoroamidate

Guidance literature:: Multi-step reaction with 4 steps

1: H₂ / Pd(OH)2/C / methanol / 48 h

2: imidazole / acetonitrile / 1 h / -5 °C

3: DMAP / pyridine / 2 h

4: TBAF, AcOH / tetrahydrofuran / 1 h

With 1H-imidazole; dmap; tetrabutyl ammonium fluoride; hydrogen; acetic acid; palladium dihydroxide; In tetrahydrofuran; pyridine; methanol; acetonitrile;
DOI:10.1016/S0040-4039(97)01122-2

Reference yield:

: 193953-64-9
C₄₇H₅₃N₂O₁₀PSi

: 193953-61-6
2,3,4-tri-O-benzoyl-α-D-glucopyranosyl tetramethylphosphoroamidate

Guidance literature:: With tetrabutyl ammonium fluoride; acetic acid; In tetrahydrofuran; for 1h;
DOI:10.1016/S0040-4039(97)01122-2

Reference yield:

: 3947-62-4,6207-76-7,19235-21-3,22554-70-7,22860-22-6,47339-09-3,57884-82-9,62057-79-8,70191-05-8,109525-54-4,140147-37-1,10343-06-3
2,3,4,5-tetra-O-acetyl-D-glucopyranose

: 193953-61-6
2,3,4-tri-O-benzoyl-α-D-glucopyranosyl tetramethylphosphoroamidate

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) n-BuLi; 2.) HMPA / tetrahydrofuran / 2 h / -10 °C

2: Et₃N / methanol / 48 h

3: imidazole / acetonitrile / 1 h / -5 °C

4: DMAP / pyridine / 2 h

5: TBAF, AcOH / tetrahydrofuran / 1 h

With 1H-imidazole; N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; n-butyllithium; tetrabutyl ammonium fluoride; acetic acid; triethylamine; In tetrahydrofuran; pyridine; methanol; acetonitrile;
DOI:10.1016/S0040-4039(97)01122-2