[2,2-Diethoxy-eth-(E)-ylidene]-((S)-2-methoxymethyl-pyrrolidin-1-yl)-amine

Base Information

Chemical Name:[2,2-Diethoxy-eth-(E)-ylidene]-((S)-2-methoxymethyl-pyrrolidin-1-yl)-amine
CAS No.:153220-75-8
Molecular Formula:C₁₂H₂₄N₂O₃
Molecular Weight:244.334
Hs Code.:

Synonyms:[2,2-Diethoxy-eth-(E)-ylidene]-((S)-2-methoxymethyl-pyrrolidin-1-yl)-amine

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Chemical Property of [2,2-Diethoxy-eth-(E)-ylidene]-((S)-2-methoxymethyl-pyrrolidin-1-yl)-amine

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Technology Process of [2,2-Diethoxy-eth-(E)-ylidene]-((S)-2-methoxymethyl-pyrrolidin-1-yl)-amine

There total 1 articles about [2,2-Diethoxy-eth-(E)-ylidene]-((S)-2-methoxymethyl-pyrrolidin-1-yl)-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 5344-23-0
diethoxyacetaldehyde

: 59983-39-0,187035-29-6
(S)-1-amino-2-(methoxymethyl)pyrrolidine

: 153220-75-8
[2,2-Diethoxy-eth-(E)-ylidene]-((S)-2-methoxymethyl-pyrrolidin-1-yl)-amine

Guidance literature:: DOI:10.1002/anie.199304181

Reference yield:

: 153220-75-8
[2,2-Diethoxy-eth-(E)-ylidene]-((S)-2-methoxymethyl-pyrrolidin-1-yl)-amine

: (R)-2,2-Diethoxy-1-phenyl-ethylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 1) CeCl₃ / 1) THF, 2 h, -78 deg C, 2) THF, a) 2 h, -100 deg C, b) 15 h, to r.t.

2: 80 percent / H₂ / Raney-nickel / methanol / 70 - 100 °C / 52504.2 Torr

With cerium(III) chloride; hydrogen; nickel; In methanol;
DOI:10.1002/anie.199304181

Reference yield:

: phenylmagnesium bromide

: 153220-75-8
[2,2-Diethoxy-eth-(E)-ylidene]-((S)-2-methoxymethyl-pyrrolidin-1-yl)-amine

: ((S)-2,2-Diethoxy-1-phenyl-ethyl)-((S)-2-methoxymethyl-pyrrolidin-1-yl)-amine

: 148402-55-5
((R)-2,2-Diethoxy-1-phenyl-ethyl)-((S)-2-methoxymethyl-pyrrolidin-1-yl)-amine

Guidance literature:: With cerium(III) chloride; Yield given. Multistep reaction. Yields of byproduct given; 1) THF, 2 h, -78 deg C, 2) THF, a) 2 h, -100 deg C, b) 15 h, to r.t.;
DOI:10.1002/anie.199304181