menthyl 6-O-benzyl-2,3,4-trideoxy-4-N-(nosylamino)-α-D-erythro-hex-2-enopyranoside

Base Information

Chemical Name:menthyl 6-O-benzyl-2,3,4-trideoxy-4-N-(nosylamino)-α-D-erythro-hex-2-enopyranoside
CAS No.:933066-50-3
Molecular Formula:C₂₉H₃₈N₂O₇S
Molecular Weight:558.696
Hs Code.:

Synonyms:menthyl 6-O-benzyl-2,3,4-trideoxy-4-N-(nosylamino)-α-D-erythro-hex-2-enopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of menthyl 6-O-benzyl-2,3,4-trideoxy-4-N-(nosylamino)-α-D-erythro-hex-2-enopyranoside

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Technology Process of menthyl 6-O-benzyl-2,3,4-trideoxy-4-N-(nosylamino)-α-D-erythro-hex-2-enopyranoside

There total 3 articles about menthyl 6-O-benzyl-2,3,4-trideoxy-4-N-(nosylamino)-α-D-erythro-hex-2-enopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 933066-41-2
6-O-benzyl-3-deoxy-3-N-(nosylamino)-4-O-mesyl-D-gulal

: 2216-51-5
(-)-menthol

: 933066-50-3
menthyl 6-O-benzyl-2,3,4-trideoxy-4-N-(nosylamino)-α-D-erythro-hex-2-enopyranoside

Guidance literature:: With potassium carbonate; In acetonitrile; at 20 ℃; for 3h;
DOI:10.1016/j.tet.2006.12.069

Reference yield:

: 933066-40-1
6-O-benzyl-3-deoxy-3-N-(nosylamino)-D-gulal

: 933066-50-3
menthyl 6-O-benzyl-2,3,4-trideoxy-4-N-(nosylamino)-α-D-erythro-hex-2-enopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / pyridine / CH₂Cl₂ / 18 h / 0 °C

2: 66 percent / K₂CO₃ / acetonitrile / 3 h / 20 °C

With pyridine; potassium carbonate; In dichloromethane; acetonitrile;
DOI:10.1016/j.tet.2006.12.069

Reference yield:

: 1694-92-4
2-Nitrobenzenesulfonyl chloride

: 933066-50-3
menthyl 6-O-benzyl-2,3,4-trideoxy-4-N-(nosylamino)-α-D-erythro-hex-2-enopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 53 percent / Et₃N / CH₂Cl₂ / 2 h / 20 °C

2: 50 percent / pyridine / CH₂Cl₂ / 18 h / 0 °C

3: 66 percent / K₂CO₃ / acetonitrile / 3 h / 20 °C

With pyridine; potassium carbonate; triethylamine; In dichloromethane; acetonitrile;
DOI:10.1016/j.tet.2006.12.069