2-methyl-5-(2,5-dimethylphenoxy)-2-pentene

Base Information

• Chemical Name: 2-methyl-5-(2,5-dimethylphenoxy)-2-pentene
• CAS No.: 172533-96-9
• Molecular Formula: C₁₄H₂₀O
• Molecular Weight: 204.312
• Mol file: 172533-96-9.mol

Synonyms:2-methyl-5-(2,5-dimethylphenoxy)-2-pentene

Chemical Property of 2-methyl-5-(2,5-dimethylphenoxy)-2-pentene

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 2-methyl-5-(2,5-dimethylphenoxy)-2-pentene

There total 4 articles about 2-methyl-5-(2,5-dimethylphenoxy)-2-pentene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.9%

5-(2,5-dimethylphenoxy)-2-methylpentan-2-ol → 2-methyl-5-(2,5-dimethylphenoxy)-2-pentene (172533-96-9)

Guidance literature:

With potassium bisulfite; 1.) from 50 to 60 deg C, 5 Torr, 5 min, 2.) from 60 to 120 deg C, 20 min;

DOI:10.1007/BF02219470

Reference yield: 55.0%

1,3-dioxoisoindolin-2-yl 5-(2,5-dimethylphenoxy)-2,2-dimethylpentanoate (1788861-30-2) → 1,4-dimethyl-2-((4-methylpent-4-en-1-yl)oxy)benzene + 2-methyl-5-(2,5-dimethylphenoxy)-2-pentene (172533-96-9)

Guidance literature:

With benzimidazole; 12-phenyl-12H-benzo[b]phenothiazine; In 1,2-dichloro-ethane; at 40 ℃; for 24h; Glovebox; Inert atmosphere; Irradiation;

DOI:10.1021/acs.orglett.1c01745

Reference yield: 52.0%

benzimidazole (271-44-3) + 1,3-dioxoisoindolin-2-yl 5-(2,5-dimethylphenoxy)-2,2-dimethylpentanoate (1788861-30-2) → 1,4-dimethyl-2-((4-methylpent-4-en-1-yl)oxy)benzene + 1-[5-(2,5-dimethylphenoxy)-2-methylpentan-2-yl]-1H-indazole + 2-methyl-5-(2,5-dimethylphenoxy)-2-pentene (172533-96-9)

Guidance literature:

With 12-phenyl-12H-benzo[b]phenothiazine; 2,4,6-trimethylpyridinium tetrafluoroborate; In 1,2-dichloro-ethane; at 40 ℃; for 24h; Glovebox; Inert atmosphere; Irradiation;

DOI:10.1021/acs.orglett.1c01745

upstream raw materials:

1,3-dioxoisoindolin-2-yl 5-(2,5-dimethylphenoxy)-2,2-dimethylpentanoate

benzimidazole

gemfibrozil

Downstream raw materials:

gemfibrozil