4,4-di-p-anisyl-2-methylthio-1-palmitoyloxy-4,5-dihydroimidazole-5-thione

Base Information

• Chemical Name: 4,4-di-p-anisyl-2-methylthio-1-palmitoyloxy-4,5-dihydroimidazole-5-thione
• CAS No.: 144267-62-9
• Molecular Formula: C₃₄H₄₈N₂O₄S₂
• Molecular Weight: 612.898

Synonyms:4,4-di-p-anisyl-2-methylthio-1-palmitoyloxy-4,5-dihydroimidazole-5-thione

Chemical Property of 4,4-di-p-anisyl-2-methylthio-1-palmitoyloxy-4,5-dihydroimidazole-5-thione

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4,4-di-p-anisyl-2-methylthio-1-palmitoyloxy-4,5-dihydroimidazole-5-thione

There total 2 articles about 4,4-di-p-anisyl-2-methylthio-1-palmitoyloxy-4,5-dihydroimidazole-5-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

4,4-di-p-anisyl-1-hydroxy-2-methylthio-4,5-dihydroimidazole-5-thione (144267-54-9) + n-hexadecanoyl chloride (112-67-4) → 4,4-di-p-anisyl-2-methylthio-1-palmitoyloxy-4,5-dihydroimidazole-5-thione (144267-62-9)

Guidance literature:

With pyridine; In dichloromethane; at 0 ℃; for 0.5h;

DOI:10.1016/S0040-4020(01)88250-8

Reference yield:

2,5-dimethylthio-4,4-di-p-anisyl-(4H)-imidazole-1-oxide (144267-41-4) → 4,4-di-p-anisyl-2-methylthio-1-palmitoyloxy-4,5-dihydroimidazole-5-thione (144267-62-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 69 percent / NaHS / dimethylformamide / 1 h / Ambient temperature

2: 93 percent / pyridine / CH₂Cl₂ / 0.5 h / 0 °C

With pyridine; sodium hydrogensulfide; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1016/S0040-4020(01)88250-8

Reference yield: 96.0%

4,4-di-p-anisyl-2-methylthio-1-palmitoyloxy-4,5-dihydroimidazole-5-thione (144267-62-9) → 4,4-di-p-anisyl-2-methylthio-5-n-pentadecylthio-(4H)-imidazole (144267-67-4)

Guidance literature:

In chloroform-d1; at 0 ℃; Irradiation;

DOI:10.1016/S0040-4020(01)88250-8

upstream raw materials:

4,4-di-p-anisyl-1-hydroxy-2-methylthio-4,5-dihydroimidazole-5-thione

n-hexadecanoyl chloride

2,5-dimethylthio-4,4-di-p-anisyl-(4H)-imidazole-1-oxide

Downstream raw materials:

4,4-di-p-anisyl-2-methylthio-5-n-pentadecylthio-(4H)-imidazole

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 144267-62-9 4,4-di-p-anisyl-2-methylthio-1-palmitoyloxy-4,5-dihydroimidazole-5-thione

Send

Send

Metric Ton KG G Pound L ML

Send

Send