5-(-N-(p-O-(N'-acetyl-(β-D-glucosaminyl)phenyl)aminocarbonyl))-2,2'-bipyridine

Base Information

• Chemical Name: 5-(-N-(p-O-(N'-acetyl-(β-D-glucosaminyl)phenyl)aminocarbonyl))-2,2'-bipyridine
• CAS No.: 1427462-45-0
• Molecular Formula: C₂₅H₂₆N₄O₇
• Molecular Weight: 494.504

Synonyms:5-(-N-(p-O-(N'-acetyl-(β-D-glucosaminyl)phenyl)aminocarbonyl))-2,2'-bipyridine

Chemical Property of 5-(-N-(p-O-(N'-acetyl-(β-D-glucosaminyl)phenyl)aminocarbonyl))-2,2'-bipyridine

Chemical Property:

Purity/Quality:

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Technology Process of 5-(-N-(p-O-(N'-acetyl-(β-D-glucosaminyl)phenyl)aminocarbonyl))-2,2'-bipyridine

There total 8 articles about 5-(-N-(p-O-(N'-acetyl-(β-D-glucosaminyl)phenyl)aminocarbonyl))-2,2'-bipyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

5-(-N-(p-O-(3,4,6-tri-O-acetyl-N'-acetyl-β-D-glucosaminyl)phenyl)aminocarbonyl)-2,2'-bipyridine (1427462-41-6) → 5-(-N-(p-O-(N'-acetyl-(β-D-glucosaminyl)phenyl)aminocarbonyl))-2,2'-bipyridine (1427462-45-0)

Guidance literature:

With sodium methylate; In tetrahydrofuran; methanol; at 20 ℃; for 2h;

DOI:10.1016/j.tet.2013.01.095

Reference yield:

Acetic acid (2R,3S,4R,5R,6R)-3-acetoxy-2-acetoxymethyl-5-acetylamino-6-chloro-tetrahydro-pyran-4-yl ester (3068-34-6) → 5-(-N-(p-O-(N'-acetyl-(β-D-glucosaminyl)phenyl)aminocarbonyl))-2,2'-bipyridine (1427462-45-0)

Guidance literature:

Multi-step reaction with 4 steps

1: tetra(n-butyl)ammonium hydroxide; sodium hydroxide / acetone / Reflux

2: hydrogen; palladium on activated charcoal / tetrahydrofuran / 20 °C

3: triethylamine / tetrahydrofuran / 0.08 h / 20 °C

4: sodium methylate / methanol; tetrahydrofuran / 2 h / 20 °C

With palladium on activated charcoal; tetra(n-butyl)ammonium hydroxide; hydrogen; sodium methylate; triethylamine; sodium hydroxide; In tetrahydrofuran; methanol; acetone;

DOI:10.1016/j.tet.2013.01.095

Reference yield:

4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) → 5-(-N-(p-O-(N'-acetyl-(β-D-glucosaminyl)phenyl)aminocarbonyl))-2,2'-bipyridine (1427462-45-0)

Guidance literature:

Multi-step reaction with 4 steps

1: tetra(n-butyl)ammonium hydroxide; sodium hydroxide / acetone / Reflux

2: hydrogen; palladium on activated charcoal / tetrahydrofuran / 20 °C

3: triethylamine / tetrahydrofuran / 0.08 h / 20 °C

4: sodium methylate / methanol; tetrahydrofuran / 2 h / 20 °C

With palladium on activated charcoal; tetra(n-butyl)ammonium hydroxide; hydrogen; sodium methylate; triethylamine; sodium hydroxide; In tetrahydrofuran; methanol; acetone;

DOI:10.1016/j.tet.2013.01.095

upstream raw materials:

Acetic acid (2R,3S,4R,5R,6R)-3-acetoxy-2-acetoxymethyl-5-acetylamino-6-chloro-tetrahydro-pyran-4-yl ester

4-nitro-phenol

p-nitrophenyl 2-acetamido-2-deoxy-3,4,6-tri-O-acetyl-β-D-glucopyranoside

6-Chloronicotinic acid methyl ester

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