7-acetoxy-4-(4'-methylphenylsulfonyl)-4-azatetracyclo<3.3.0.0^2,8.0^3,6>octane

Base Information

• Chemical Name: 7-acetoxy-4-(4'-methylphenylsulfonyl)-4-azatetracyclo<3.3.0.0^2,8.0^3,6>octane
• CAS No.: 136708-53-7
• Molecular Formula: C₁₆H₁₇NO₄S
• Molecular Weight: 319.381

Synonyms:7-acetoxy-4-(4'-methylphenylsulfonyl)-4-azatetracyclo<3.3.0.0^2,8.0^3,6>octane

Chemical Property of 7-acetoxy-4-(4'-methylphenylsulfonyl)-4-azatetracyclo<3.3.0.0^2,8.0^3,6>octane

Chemical Property:

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Technology Process of 7-acetoxy-4-(4'-methylphenylsulfonyl)-4-azatetracyclo<3.3.0.0^2,8.0^3,6>octane

There total 1 articles about 7-acetoxy-4-(4'-methylphenylsulfonyl)-4-azatetracyclo<3.3.0.0^2,8.0^3,6>octane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-toluenesulfonyl azide (941-55-9) + 7-acetoxynorbornadiene (13426-49-8) → Acetic acid (1R,5R,8S)-2-(toluene-4-sulfonyl)-2-aza-bicyclo[3.2.1]octa-3,6-dien-8-yl ester (136708-54-8) + 7-acetoxy-4-(4'-methylphenylsulfonyl)-4-azatetracyclo<3.3.0.02,8.03,6>octane (136708-53-7)

Guidance literature:

In methanol; for 432h; Yield given. Yields of byproduct given; Ambient temperature;

Reference yield: 88.0%

7-acetoxy-4-(4'-methylphenylsulfonyl)-4-azatetracyclo<3.3.0.02,8.03,6>octane (136708-53-7) → 7-hydroxy-4-(4'-methylphenylsulfonyl)-4-tetracyclo<3.3.0.02,8.03,6>octane (136708-83-3)

Guidance literature:

With potassium hydroxide; In ethanol; at 0 ℃;

Reference yield: 36.0%

7-acetoxy-4-(4'-methylphenylsulfonyl)-4-azatetracyclo<3.3.0.02,8.03,6>octane (136708-53-7) → N-(exo-6-formylbicyclo<3.1.0>hex-3-en-exo-2-yl)-p-toluenesulfonamide (136708-82-2)

Guidance literature:

With potassium hydroxide; In ethanol; for 2.5h;

upstream raw materials:

4-toluenesulfonyl azide

7-acetoxynorbornadiene

Downstream raw materials:

N-(exo-6-formylbicyclo<3.1.0>hex-3-en-exo-2-yl)-p-toluenesulfonamide

7-hydroxy-4-(4'-methylphenylsulfonyl)-4-tetracyclo<3.3.0.0^2,8.0^3,6>octane

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