tert-Butyl 1-(5-(3-bromophenyl)-1H-1,2,4-triazol-3-yl)cyclopentylcarbamate

Base Information

• Chemical Name: tert-Butyl 1-(5-(3-bromophenyl)-1H-1,2,4-triazol-3-yl)cyclopentylcarbamate
• CAS No.: 877285-74-0
• Molecular Formula: C₁₈H₂₃BrN₄O₂
• Molecular Weight: 407.31
• Mol file: 877285-74-0.mol

Synonyms:tert-Butyl 1-(5-(3-bromophenyl)-1H-1,2,4-triazol-3-yl)cyclopentylcarbamate

Chemical Property of tert-Butyl 1-(5-(3-bromophenyl)-1H-1,2,4-triazol-3-yl)cyclopentylcarbamate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of tert-Butyl 1-(5-(3-bromophenyl)-1H-1,2,4-triazol-3-yl)cyclopentylcarbamate

There total 1 articles about tert-Butyl 1-(5-(3-bromophenyl)-1H-1,2,4-triazol-3-yl)cyclopentylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

1-[[(1,1-dimethylethoxy)carbonyl]amino]-cyclopentanecarboxylic acid hydrazide (877285-67-1) + 3-bromobenzenecarboximidic acid ethyl ester monohydrochloride (57508-63-1) → tert-Butyl 1-(5-(3-bromophenyl)-1H-1,2,4-triazol-3-yl)cyclopentylcarbamate (877285-74-0)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In isopropyl alcohol; at 20 - 65 ℃; for 120h;

Reference yield: 73.0%

tert-Butyl 1-(5-(3-bromophenyl)-1H-1,2,4-triazol-3-yl)cyclopentylcarbamate (877285-74-0) + acrylic acid methyl ester (292638-85-8,9003-21-8,96-33-3) → C22H28N4O4

Guidance literature:

With N-ethyl-N,N-diisopropylamine; palladium diacetate; tris-(o-tolyl)phosphine; In acetonitrile; at 120 - 170 ℃; for 0.25h; microwave;

upstream raw materials:

1-[[(1,1-dimethylethoxy)carbonyl]amino]-cyclopentanecarboxylic acid hydrazide

3-bromobenzenecarboximidic acid ethyl ester monohydrochloride