ethyl 3-bromobenzenecarboximidoate hydrochloride

Base Information

• Chemical Name: ethyl 3-bromobenzenecarboximidoate hydrochloride
• CAS No.: 57508-63-1
• Molecular Formula: C9H11BrClNO
• Molecular Weight: 264.549
• Mol file: 57508-63-1.mol

Synonyms:ethyl 3-bromobenzenecarboximidoate hydrochloride;ethyl3-broMobenziMidatehydrochloride

Chemical Property of ethyl 3-bromobenzenecarboximidoate hydrochloride

Chemical Property:

• PSA: 33.08000
• LogP: 3.71270

Purity/Quality:

99% ^*data from raw suppliers

3-Bromobenzimidic acid ethyl ester hydrochloride 90%+ ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ethyl 3-bromobenzenecarboximidoate hydrochloride

There total 1 articles about ethyl 3-bromobenzenecarboximidoate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

ethanol (64-17-5) + 3-cyanobromobenzene (6952-59-6) → 3-bromobenzenecarboximidic acid ethyl ester monohydrochloride (57508-63-1)

Guidance literature:

With hydrogenchloride; In ethanol;

Reference yield: 100.0%

3-bromobenzenecarboximidic acid ethyl ester monohydrochloride (57508-63-1) + benzoyl chloride (98-88-4) → ethyl (Z)-N-benzoyl-3-bromobenzimidate

Guidance literature:

With triethylamine; In dichloromethane; at 30 - 40 ℃; for 6h;

Reference yield: 93.0%

3-bromobenzenecarboximidic acid ethyl ester monohydrochloride (57508-63-1) + butyryl chloride (141-75-3) → C13H16BrNO2 (1415127-42-2)

Guidance literature:

3-bromobenzenecarboximidic acid ethyl ester monohydrochloride; With triethylamine; In toluene; at 20 ℃; for 0.166667h;

butyryl chloride; In toluene; at 20 ℃; for 24h;

upstream raw materials:

ethanol

3-cyanobromobenzene

Downstream raw materials:

tert-Butyl 1-(5-(3-bromophenyl)-1H-1,2,4-triazol-3-yl)cyclopentylcarbamate

C₁₃H₁₆BrNO₂

3-(3-bromophenyl)-1-(2-methylphenyl)-5-propyl-1H-1,2,4-triazole

3-(biphenyl-3-yl)-1-(2-methylphenyl)-5-propyl-1H-1,2,4-triazole