C₄₃H₅₂O₉

Base Information

Chemical Name:C₄₃H₅₂O₉
CAS No.:1265446-85-2
Molecular Formula:C₄₃H₅₂O₉
Molecular Weight:712.88
Hs Code.:

C<sub>43</sub>H<sub>52</sub>O<sub>9</sub>

Synonyms:C₄₃H₅₂O₉

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Chemical Property of C₄₃H₅₂O₉

Chemical Property:

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Technology Process of C₄₃H₅₂O₉

There total 7 articles about C₄₃H₅₂O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₂H₅₀O₁₀

: 1779-49-3
Methyltriphenylphosphonium bromide

: 1265446-85-2
C₄₃H₅₂O₉

Guidance literature:: Methyltriphenylphosphonium bromide; With potassium tert-butylate; In tetrahydrofuran; at 0 ℃; for 0.5h;

C₄₂H₅₀O₁₀; In tetrahydrofuran; at 0 ℃; for 1h;
DOI:10.1021/np100729d

Reference yield:

: 1265446-63-6
C₇₀H₈₀O₁₁SSeSi

: 1265446-85-2
C₄₃H₅₂O₉

Guidance literature:: Multi-step reaction with 6 steps

1.1: triethyl borane; tri-n-butyl-tin hydride / tetrahydrofuran; toluene / 5 h / -40 - -15 °C / in air

2.1: pyridine; trifluoroacetic anhydride / acetonitrile / 7 h / 0 °C

3.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 0 °C

3.2: 0.5 h / 0 °C

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C

5.1: Dess-Martin periodane / dichloromethane / 1.5 h / 20 °C

6.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 0 °C

6.2: 1 h / 0 °C

With pyridine; triethyl borane; potassium tert-butylate; tetrabutyl ammonium fluoride; tri-n-butyl-tin hydride; Dess-Martin periodane; trifluoroacetic anhydride; In tetrahydrofuran; dichloromethane; toluene; acetonitrile; 2.1: Pummerer reaction / 2.2: Pummerer reaction / 3.1: Wittig reaction / 3.2: Wittig reaction / 6.1: Wittig reaction / 6.2: Wittig reaction;
DOI:10.1021/np100729d

Reference yield:

: 1265446-53-4
C₆₇H₈₆O₁₀SeSi₂

: 1265446-85-2
C₄₃H₅₂O₉

Guidance literature:: Multi-step reaction with 8 steps

1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / -30 - 0 °C

2.1: methyllithium / tetrahydrofuran; diethyl ether / -78 - 20 °C

2.2: Inert atmosphere

3.1: triethyl borane; tri-n-butyl-tin hydride / tetrahydrofuran; toluene / 5 h / -40 - -15 °C / in air

4.1: pyridine; trifluoroacetic anhydride / acetonitrile / 7 h / 0 °C

5.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 0 °C

5.2: 0.5 h / 0 °C

6.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C

7.1: Dess-Martin periodane / dichloromethane / 1.5 h / 20 °C

8.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 0 °C

8.2: 1 h / 0 °C

With pyridine; triethyl borane; potassium tert-butylate; tetrabutyl ammonium fluoride; methyllithium; tri-n-butyl-tin hydride; Dess-Martin periodane; trifluoroacetic anhydride; In tetrahydrofuran; diethyl ether; dichloromethane; toluene; acetonitrile; 4.1: Pummerer reaction / 4.2: Pummerer reaction / 5.1: Wittig reaction / 5.2: Wittig reaction / 8.1: Wittig reaction / 8.2: Wittig reaction;
DOI:10.1021/np100729d