1-O-(p-methoxyphenyl)-2,3-di-O-acetyl-6-O-levulinoyl-β-D-glucopyranoside

Base Information

Chemical Name:1-O-(p-methoxyphenyl)-2,3-di-O-acetyl-6-O-levulinoyl-β-D-glucopyranoside
CAS No.:1140306-45-1
Molecular Formula:C₂₂H₂₈O₁₁
Molecular Weight:468.458
Hs Code.:

Synonyms:1-O-(p-methoxyphenyl)-2,3-di-O-acetyl-6-O-levulinoyl-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-O-(p-methoxyphenyl)-2,3-di-O-acetyl-6-O-levulinoyl-β-D-glucopyranoside

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Technology Process of 1-O-(p-methoxyphenyl)-2,3-di-O-acetyl-6-O-levulinoyl-β-D-glucopyranoside

There total 1 articles about 1-O-(p-methoxyphenyl)-2,3-di-O-acetyl-6-O-levulinoyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1140306-42-8
4-methoxyphenyl 2,3-di-O-acetyl-β-D-glucopyranoside

: 123-76-2
levulinic acid

: 1140306-45-1
1-O-(p-methoxyphenyl)-2,3-di-O-acetyl-6-O-levulinoyl-β-D-glucopyranoside

Guidance literature:: 4-methoxyphenyl 2,3-di-O-acetyl-β-D-glucopyranoside; levulinic acid; With 2-chloro-1-methyl-pyridinium iodide; In dichloromethane; at 20 ℃; for 0.25h;

With 1,4-diaza-bicyclo[2.2.2]octane; In dichloromethane; for 1h;

Reference yield: 78.0%

: 1140306-45-1
1-O-(p-methoxyphenyl)-2,3-di-O-acetyl-6-O-levulinoyl-β-D-glucopyranoside

: 541-88-8
Chloroacetic anhydride

: 1140306-48-4
1-O-(p-methoxyphenyl)-2,3-di-O-acetyl-4-O-chloroacetyl-6-O-levulinoyl-β-D-glucopyranoside

Guidance literature:: With pyridine; In dichloromethane; at 0 ℃; for 0.5h;

Reference yield: 55.0%

: 1140306-45-1
1-O-(p-methoxyphenyl)-2,3-di-O-acetyl-6-O-levulinoyl-β-D-glucopyranoside

: 1140307-16-9
2-deoxy-2-trichloroacetamido-3-O-chloroacetyl-4,6-O-benzylidene-α-D-glucopyranosyl trichloroacetimidate

: 1140307-19-2
p-methoxyphenyl-(2-deoxy-2-trichloroacetamido-4,6-O-benzylidene-β-D-glucopyranosyl)-(1-4)-O-(2,3-di-O-acetyl-6-O-levulinoyl-β-D-glucopyranoside)

Guidance literature:: 1-O-(p-methoxyphenyl)-2,3-di-O-acetyl-6-O-levulinoyl-β-D-glucopyranoside; 2-deoxy-2-trichloroacetamido-3-O-chloroacetyl-4,6-O-benzylidene-α-D-glucopyranosyl trichloroacetimidate; In dichloromethane; at 20 ℃; for 0.25h; Molecular sieve;

With boron trifluoride diethyl etherate; In dichloromethane; at 0 ℃; for 1h;