C₁₄H₂₂O₃

Base Information

• Chemical Name: C₁₄H₂₂O₃
• CAS No.: 1428957-02-1
• Molecular Formula: C₁₄H₂₂O₃
• Molecular Weight: 238.327
• Mol file: 1428957-02-1.mol

Synonyms:C₁₄H₂₂O₃

Chemical Property of C₁₄H₂₂O₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₄H₂₂O₃

There total 3 articles about C₁₄H₂₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyl cyclohexylideneacetate (1552-92-7) → C14H22O3 (1428957-02-1)

Guidance literature:

Multi-step reaction with 3 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Inert atmosphere

2.1: phosphorus tribromide / diethyl ether / 0 °C / Inert atmosphere

3.1: sodium ethanolate / ethanol / 0 °C

3.2: 16 h / 0 - 20 °C

With lithium aluminium tetrahydride; sodium ethanolate; phosphorus tribromide; In tetrahydrofuran; diethyl ether; ethanol;

Reference yield:

cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) → C14H22O3 (1428957-02-1)

Guidance literature:

Multi-step reaction with 4 steps

1.1: sodium hydride; 15-crown-5 / tetrahydrofuran; mineral oil / 0 °C

1.2: -40 - 20 °C

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Inert atmosphere

3.1: phosphorus tribromide / diethyl ether / 0 °C / Inert atmosphere

4.1: sodium ethanolate / ethanol / 0 °C

4.2: 16 h / 0 - 20 °C

With lithium aluminium tetrahydride; 15-crown-5; sodium ethanolate; phosphorus tribromide; sodium hydride; In tetrahydrofuran; diethyl ether; ethanol; mineral oil;

Reference yield:

2-cyclohexylidene ethanol (932-89-8) → C14H22O3 (1428957-02-1)

Guidance literature:

Multi-step reaction with 2 steps

1.1: phosphorus tribromide / diethyl ether / 0 °C / Inert atmosphere

2.1: sodium ethanolate / ethanol / 0 °C

2.2: 16 h / 0 - 20 °C

With sodium ethanolate; phosphorus tribromide; In diethyl ether; ethanol;

upstream raw materials:

cyclohexanone

ethyl cyclohexylideneacetate

2-cyclohexylidene ethanol

Downstream raw materials:

5-cyclohexylidene-pentan-2-one

(E)-6-cyclohexylidene-3-methylhex-2-en-1-ol

(E)-ethyl 2-acetyl-8-cyclohexylidene-5-methyloct-4-enoate

(E)-9-Cyclohexylidene-6-methyl-non-5-en-2-one