1,6-dichloro-4-phenylphthalazine

Base Information Edit

Chemical Name:1,6-dichloro-4-phenylphthalazine
CAS No.:120116-66-7
Molecular Formula:C₁₄H₈Cl₂N₂
Molecular Weight:275.137
Hs Code.:
Mol file:120116-66-7.mol

Synonyms:1,6-dichloro-4-phenylphthalazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,6-dichloro-4-phenylphthalazine Edit

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Technology Process of 1,6-dichloro-4-phenylphthalazine

There total 2 articles about 1,6-dichloro-4-phenylphthalazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 33184-56-4
2-benzoyl-4-chlorobenzoic acid

: 120116-66-7
1,6-dichloro-4-phenylphthalazine

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / hydrazine hydrate / ethanol / 1 h / Heating

2: 1.) phosphorus oxychloride; 2.) conc. ammonium hydroxide / 1.) 1 h, 100 degC; 2.) 20 degC, pH=7.8; 10 min

With ammonium hydroxide; hydrazine hydrate; trichlorophosphate; In ethanol;

Reference yield:

: 120116-65-6
6-chloro-4-phenylphthalazine-1(2H)-one

: 120116-66-7
1,6-dichloro-4-phenylphthalazine

Guidance literature:: With ammonium hydroxide; trichlorophosphate; Yield given. Multistep reaction; 1.) 1 h, 100 degC; 2.) 20 degC, pH=7.8; 10 min;