bis[2,6-bis(1,1,1,3,3,3-hexafluoroisopropoxymethyl)-4-tert-butylphenyl] disulfide

Base Information

Chemical Name:bis[2,6-bis(1,1,1,3,3,3-hexafluoroisopropoxymethyl)-4-tert-butylphenyl] disulfide
CAS No.:1259293-83-8
Molecular Formula:C₃₆H₃₄F₂₄O₄S₂
Molecular Weight:1050.76
Hs Code.:

Synonyms:bis[2,6-bis(1,1,1,3,3,3-hexafluoroisopropoxymethyl)-4-tert-butylphenyl] disulfide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis[2,6-bis(1,1,1,3,3,3-hexafluoroisopropoxymethyl)-4-tert-butylphenyl] disulfide

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Technology Process of bis[2,6-bis(1,1,1,3,3,3-hexafluoroisopropoxymethyl)-4-tert-butylphenyl] disulfide

There total 4 articles about bis[2,6-bis(1,1,1,3,3,3-hexafluoroisopropoxymethyl)-4-tert-butylphenyl] disulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 920-66-1
1,1,1,3',3',3'-hexafluoro-propanol

: 1259294-21-7
bis[2,6-bis(bromomethyl)-4-tert-butylphenyl] disulfide

: 1259293-83-8
bis[2,6-bis(1,1,1,3,3,3-hexafluoroisopropoxymethyl)-4-tert-butylphenyl] disulfide

Guidance literature:: 1,1,1,3',3',3'-hexafluoro-propanol; With potassium hydride; In hexane; Inert atmosphere;

bis[2,6-bis(bromomethyl)-4-tert-butylphenyl] disulfide; In hexane; toluene; at 110 ℃; for 30h; Inert atmosphere;
DOI:10.1021/ja106343h

Reference yield:

: 1006064-11-4
bis[4-tert-butyl-2,6-bis(methoxymethyl)phenyl] disulfide

: 1259293-83-8
bis[2,6-bis(1,1,1,3,3,3-hexafluoroisopropoxymethyl)-4-tert-butylphenyl] disulfide

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogen bromide; acetic acid / 4 h / 65 °C

2.1: potassium hydride / hexane / Inert atmosphere

2.2: 30 h / 110 °C / Inert atmosphere

With hydrogen bromide; potassium hydride; acetic acid; In hexane;
DOI:10.1021/ja106343h

Reference yield:

: 287969-13-5
2-bromo-5-tert-butyl-1,3-bis(methoxymethyl)benzene

: 1259293-83-8
bis[2,6-bis(1,1,1,3,3,3-hexafluoroisopropoxymethyl)-4-tert-butylphenyl] disulfide

Guidance literature:: Multi-step reaction with 3 steps

1.1: iodine; magnesium / tetrahydrofuran / 2 h / Reflux; Inert atmosphere

1.2: 2 h / Cooling with ice; Reflux; Inert atmosphere

1.3: Cooling with ice

2.1: hydrogen bromide; acetic acid / 4 h / 65 °C

3.1: potassium hydride / hexane / Inert atmosphere

3.2: 30 h / 110 °C / Inert atmosphere

With hydrogen bromide; iodine; potassium hydride; magnesium; acetic acid; In tetrahydrofuran; hexane;
DOI:10.1021/ja106343h