Technology Process of C47H30N6
There total 8 articles about C47H30N6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C32H21N3;
With
sodium hydride;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 0.5h;
Inert atmosphere;
2-chloro-4,6-diphenyl-1,3,5-triazine;
In
N,N-dimethyl-formamide;
at 60 ℃;
for 0.5h;
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: sodium hydride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere
1.2: 1.5 h / 20 °C / Inert atmosphere
2.1: N-Bromosuccinimide / tetrahydrofuran / 2.5 h / 20 °C / Inert atmosphere
3.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -60 °C / Inert atmosphere
3.2: 1 h
4.1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / water; toluene; ethanol / 90 °C
5.1: tetra-n-butylammoniumfluoride trihydrate / tetrahydrofuran / 1 h / 20 °C
6.1: copper(l) iodide; potassium phosphate; trans cyclohexane-1,2-diamine / 1,4-dioxane / 10 h / 120 °C
7.1: triethyl phosphite; Isopropylbenzene / 17 h / 160 °C
8.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere
8.2: 0.5 h / 60 °C
With
potassium phosphate; N-Bromosuccinimide; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); n-butyllithium; Isopropylbenzene; trans cyclohexane-1,2-diamine; sodium hydride; sodium carbonate; tetra-n-butylammoniumfluoride trihydrate; triethyl phosphite;
In
tetrahydrofuran; 1,4-dioxane; ethanol; hexane; water; N,N-dimethyl-formamide; toluene;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -60 °C / Inert atmosphere
1.2: 1 h
2.1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / water; toluene; ethanol / 90 °C
3.1: tetra-n-butylammoniumfluoride trihydrate / tetrahydrofuran / 1 h / 20 °C
4.1: copper(l) iodide; potassium phosphate; trans cyclohexane-1,2-diamine / 1,4-dioxane / 10 h / 120 °C
5.1: triethyl phosphite; Isopropylbenzene / 17 h / 160 °C
6.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere
6.2: 0.5 h / 60 °C
With
potassium phosphate; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); n-butyllithium; Isopropylbenzene; trans cyclohexane-1,2-diamine; sodium hydride; sodium carbonate; tetra-n-butylammoniumfluoride trihydrate; triethyl phosphite;
In
tetrahydrofuran; 1,4-dioxane; ethanol; hexane; water; N,N-dimethyl-formamide; toluene;