Technology Process of p-nitrophenyl carbonate quadricyclane
There total 4 articles about p-nitrophenyl carbonate quadricyclane which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridine;
In
dichloromethane;
at 0 - 20 ℃;
for 3h;
DOI:10.1021/ja2072934
- Guidance literature:
-
Multi-step reaction with 4 steps
1: perchloric acid / acetic acid / 0.02 h / 0 °C
2: hexane; acetone / 5 h / Irradiation; Inert atmosphere
3: lithium aluminium tetrahydride / diethyl ether / 0 - 20 °C
4: pyridine / dichloromethane / 3 h / 0 - 20 °C
With
pyridine; lithium aluminium tetrahydride; perchloric acid;
In
diethyl ether; hexane; dichloromethane; acetic acid; acetone;
DOI:10.1021/ja2072934
- Guidance literature:
-
Multi-step reaction with 3 steps
1: hexane; acetone / 5 h / Irradiation; Inert atmosphere
2: lithium aluminium tetrahydride / diethyl ether / 0 - 20 °C
3: pyridine / dichloromethane / 3 h / 0 - 20 °C
With
pyridine; lithium aluminium tetrahydride;
In
diethyl ether; hexane; dichloromethane; acetone;
DOI:10.1021/ja2072934
