3-benzoylphenyl trifluoromethanesulfonate

Base Information

• Chemical Name: 3-benzoylphenyl trifluoromethanesulfonate
• CAS No.: 209917-31-7
• Molecular Formula: C₁₄H₉F₃O₄S
• Molecular Weight: 330.284
• Mol file: 209917-31-7.mol

Synonyms:3-benzoylphenyl trifluoromethanesulfonate

Chemical Property of 3-benzoylphenyl trifluoromethanesulfonate

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 3-benzoylphenyl trifluoromethanesulfonate

There total 2 articles about 3-benzoylphenyl trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

trifluoromethylsulfonic anhydride (358-23-6) + 3-hydroxybenzophenone (13020-57-0) → 3-benzoylphenyl trifluoromethanesulfonate (209917-31-7)

Guidance literature:

With pyridine; In dichloromethane; at 0 - 25 ℃; Inert atmosphere;

DOI:10.1021/ja2066829

Reference yield: 93.0%

→ 3-benzoylphenyl trifluoromethanesulfonate (209917-31-7)

Guidance literature:

With pyridine; In dichloromethane; at 0 - 25 ℃; for 5h; Inert atmosphere;

Reference yield: 89.0%

3-benzoylphenyl trifluoromethanesulfonate (209917-31-7) + cyclohexene (110-83-8) → 1-(m-benzoylphenyl)cyclohexene

Guidance literature:

With 1,2-dimethoxybenzene; bis(1,1,1,5,5,5-hexafluoro-2,4-pentanedionato)palladium(II); 1,3-bis-(diphenylphosphino)propane; lithium carbonate; at 120 ℃; for 48h; Inert atmosphere;

DOI:10.1002/chem.201204427

upstream raw materials:

trifluoromethylsulfonic anhydride

3-hydroxybenzophenone

Downstream raw materials:

3-(2-methylphenyl)benzophenone

3-(2'-(hydroxymethyl)phenyl)benzophenone

(S)-tert-butyl 2-(3'-benzoylphenyl)propionate