N-((6-(2-benzyloxyethoxy)-4'-methylbiphenyl)-2-yl)-4-tert-butylbenzenesulfonamide

Base Information

Chemical Name:N-((6-(2-benzyloxyethoxy)-4'-methylbiphenyl)-2-yl)-4-tert-butylbenzenesulfonamide
CAS No.:374601-16-8
Molecular Formula:C₃₂H₃₅NO₄S
Molecular Weight:529.7
Hs Code.:

Synonyms:N-((6-(2-benzyloxyethoxy)-4'-methylbiphenyl)-2-yl)-4-tert-butylbenzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-((6-(2-benzyloxyethoxy)-4'-methylbiphenyl)-2-yl)-4-tert-butylbenzenesulfonamide

Chemical Property:

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Technology Process of N-((6-(2-benzyloxyethoxy)-4'-methylbiphenyl)-2-yl)-4-tert-butylbenzenesulfonamide

There total 5 articles about N-((6-(2-benzyloxyethoxy)-4'-methylbiphenyl)-2-yl)-4-tert-butylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 15084-51-2
4-tert-butylbenzenesulfonyl chloride

: 374601-14-6
6-(2-benzyloxyethoxy)-4'-methylbiphenyl-2-amine

: 374601-16-8
N-((6-(2-benzyloxyethoxy)-4'-methylbiphenyl)-2-yl)-4-tert-butylbenzenesulfonamide

Guidance literature:: With pyridine; at 20 ℃; for 2h;
DOI:10.1021/jm0102304

Reference yield:

: 622-08-2,1201808-31-2
2-Benzyloxyethanol

: 374601-16-8
N-((6-(2-benzyloxyethoxy)-4'-methylbiphenyl)-2-yl)-4-tert-butylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / PPh₃; DEAD / tetrahydrofuran / 2 h / 0 °C

2: 89 percent / PdCl₂(PPh₃)2 / dioxane / 4 h / 20 °C

3: 87 percent / Fe; 10percent aq. HCl / ethanol / 3.5 h / Heating

4: 100 percent / pyridine / 2 h / 20 °C

With pyridine; bis-triphenylphosphine-palladium(II) chloride; iron; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; 1,4-dioxane; ethanol;
DOI:10.1021/jm0102304

Reference yield:

: 603-84-9
2-chloro-3-nitrophenol

: 374601-16-8
N-((6-(2-benzyloxyethoxy)-4'-methylbiphenyl)-2-yl)-4-tert-butylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / PPh₃; DEAD / tetrahydrofuran / 2 h / 0 °C

2: 89 percent / PdCl₂(PPh₃)2 / dioxane / 4 h / 20 °C

3: 87 percent / Fe; 10percent aq. HCl / ethanol / 3.5 h / Heating

4: 100 percent / pyridine / 2 h / 20 °C

With pyridine; bis-triphenylphosphine-palladium(II) chloride; iron; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; 1,4-dioxane; ethanol;
DOI:10.1021/jm0102304