C₄₂H₄₃FO₄

Base Information

Chemical Name:C₄₂H₄₃FO₄
CAS No.:1181680-83-0
Molecular Formula:C₄₂H₄₃FO₄
Molecular Weight:630.799
Hs Code.:

C<sub>42</sub>H<sub>43</sub>FO<sub>4</sub>

Synonyms:C₄₂H₄₃FO₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₂H₄₃FO₄

Chemical Property:

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Technology Process of C₄₂H₄₃FO₄

There total 13 articles about C₄₂H₄₃FO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: C₄₂H₄₃FO₅

: 1181680-83-0
C₄₂H₄₃FO₄

Guidance literature:: With triethylsilane; boron trifluoride diethyl etherate; In acetonitrile; at -40 ℃; for 0.5h; Inert atmosphere;

Reference yield:

: 10257-28-0
D-Galactose

: 1181680-83-0
C₄₂H₄₃FO₄

Guidance literature:: Multi-step reaction with 12 steps

1.1: pyridine / dmap / dichloromethane / 3.33 h / 35 °C / Reflux

2.1: triethylamine / dmap / dichloromethane

3.1: BAST / tetrahydrofuran / 2 h / 20 °C / Cooling with water

4.1: hydrogen bromide; acetic acid / 1 h / 20 °C

5.1: potassium carbonate / dichloromethane; N,N-dimethyl-formamide / 2 h / 20 °C

6.1: sodium methylate / methanol / 12 h / Reflux

7.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 2 h / 20 °C

8.1: N-Bromosuccinimide / acetone / 2 h / 20 °C

9.1: water / ethyl acetate

10.1: acetic anhydride / dimethyl sulfoxide / 20 °C

11.1: n-butyllithium / toluene; tetrahydrofuran / 0.17 h / -78 °C / Inert atmosphere

11.2: 0.5 h / -78 °C

12.1: boron trifluoride diethyl etherate; triethylsilane / acetonitrile / 0.5 h / -40 °C / Inert atmosphere

With pyridine; triethylsilane; N-Bromosuccinimide; n-butyllithium; boron trifluoride diethyl etherate; water; hydrogen bromide; sodium methylate; acetic anhydride; sodium hydride; potassium carbonate; acetic acid; triethylamine; dmap; In tetrahydrofuran; methanol; dichloromethane; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide; acetone; toluene; acetonitrile; mineral oil;

Reference yield:

: 1,3,6-tri-O-pivaloyl-β-D-galactopyranose

: 1181680-83-0
C₄₂H₄₃FO₄

Guidance literature:: Multi-step reaction with 11 steps

1.1: triethylamine / dmap / dichloromethane

2.1: BAST / tetrahydrofuran / 2 h / 20 °C / Cooling with water

3.1: hydrogen bromide; acetic acid / 1 h / 20 °C

4.1: potassium carbonate / dichloromethane; N,N-dimethyl-formamide / 2 h / 20 °C

5.1: sodium methylate / methanol / 12 h / Reflux

6.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 2 h / 20 °C

7.1: N-Bromosuccinimide / acetone / 2 h / 20 °C

8.1: water / ethyl acetate

9.1: acetic anhydride / dimethyl sulfoxide / 20 °C

10.1: n-butyllithium / toluene; tetrahydrofuran / 0.17 h / -78 °C / Inert atmosphere

10.2: 0.5 h / -78 °C

11.1: boron trifluoride diethyl etherate; triethylsilane / acetonitrile / 0.5 h / -40 °C / Inert atmosphere

With triethylsilane; N-Bromosuccinimide; n-butyllithium; boron trifluoride diethyl etherate; water; hydrogen bromide; sodium methylate; acetic anhydride; sodium hydride; potassium carbonate; acetic acid; triethylamine; dmap; In tetrahydrofuran; methanol; dichloromethane; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide; acetone; toluene; acetonitrile; mineral oil;