1,3-Dibenzyl-2-(4,4-dimethyl-2-methylsulfanyl-6-thioxo-cyclohex-1-enyl)-4,5-dihydro-3H-imidazol-1-ium; iodide

Base Information

• Chemical Name: 1,3-Dibenzyl-2-(4,4-dimethyl-2-methylsulfanyl-6-thioxo-cyclohex-1-enyl)-4,5-dihydro-3H-imidazol-1-ium; iodide
• CAS No.: 115094-73-0
• Molecular Formula: C₂₆H₃₁N₂S₂*I
• Molecular Weight: 562.582

Synonyms:1,3-Dibenzyl-2-(4,4-dimethyl-2-methylsulfanyl-6-thioxo-cyclohex-1-enyl)-4,5-dihydro-3H-imidazol-1-ium; iodide

Chemical Property of 1,3-Dibenzyl-2-(4,4-dimethyl-2-methylsulfanyl-6-thioxo-cyclohex-1-enyl)-4,5-dihydro-3H-imidazol-1-ium; iodide

Chemical Property:

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Technology Process of 1,3-Dibenzyl-2-(4,4-dimethyl-2-methylsulfanyl-6-thioxo-cyclohex-1-enyl)-4,5-dihydro-3H-imidazol-1-ium; iodide

There total 1 articles about 1,3-Dibenzyl-2-(4,4-dimethyl-2-methylsulfanyl-6-thioxo-cyclohex-1-enyl)-4,5-dihydro-3H-imidazol-1-ium; iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,3-dibenzyl-2-(4,4-dimethyl-2,5-bisthioxocyclohexylidene)imidazolidine (103681-73-8) + methyl iodide (74-88-4) → 1,3-Dibenzyl-2-(4,4-dimethyl-2-methylsulfanyl-6-thioxo-cyclohex-1-enyl)-4,5-dihydro-3H-imidazol-1-ium; iodide (115094-73-0)

Guidance literature:

In acetone; Yield given;

DOI:10.1021/jo00005a043

Reference yield: 98.0%

1,3-Dibenzyl-2-(4,4-dimethyl-2-methylsulfanyl-6-thioxo-cyclohex-1-enyl)-4,5-dihydro-3H-imidazol-1-ium; iodide (115094-73-0) → 1,3-Dibenzyl-2-<2-(methyl)thio-4,4-dimethyl-6-thioxo-cyclohex-2-enylidene>imidazolidine

Guidance literature:

With sodium hydrogencarbonate; In acetone;

DOI:10.1021/jo00005a043

Reference yield:

1,3-Dibenzyl-2-(4,4-dimethyl-2-methylsulfanyl-6-thioxo-cyclohex-1-enyl)-4,5-dihydro-3H-imidazol-1-ium; iodide (115094-73-0) → 4--amino>-5-(methylthio)-7H-7,7-dimethylbenzothiopyran-2,3-dicarboxylate (115094-79-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 98 percent / 5percent aq. NaHCO₃ / acetone

2: 13 percent / silica gel / CH₂Cl₂

With sodium hydrogencarbonate; silica gel; In dichloromethane; acetone;

DOI:10.1021/jo00005a043

upstream raw materials:

1,3-dibenzyl-2-(4,4-dimethyl-2,5-bisthioxocyclohexylidene)imidazolidine

methyl iodide

Downstream raw materials:

2,3-Bis(methoxycarbonyl)-7,8-dihydro-5-(methylthio)-7,7-dimethyl-1',3'-dibenzyl-4H-benzothiopyran-4-spiro-2'-imidazolidine

4--amino>-5-(methylthio)-7H-7,7-dimethylbenzothiopyran-2,3-dicarboxylate

Dimethyl 4-amino>ethyl>amino>5-(methylthio)-7H-7,7,-dimethylbenzothiopyran-2,3-dicarboxylate

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