Technology Process of C19H21ClN4O3
There total 6 articles about C19H21ClN4O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
acetonitrile;
at 0 - 20 ℃;
for 2h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: carbonochloridic acid 1-chloro-ethyl ester / 1,2-dichloro-ethane / 16.25 h / 0 - 20 °C
2: triethylamine / dichloromethane / 16 h / 0 - 20 °C
3: ruthenium tetroxide; sodium periodate / water; ethyl acetate / 16 h / 0 - 20 °C
4: acetonitrile / 2 h / 0 - 20 °C
With
sodium periodate; ruthenium tetroxide; carbonochloridic acid 1-chloro-ethyl ester; triethylamine;
In
dichloromethane; water; ethyl acetate; 1,2-dichloro-ethane; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: sodium methylate / methanol / 96 h / 0 - 60 °C / Inert atmosphere
2: trichlorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 2 h / 0 - 130 °C
3: carbonochloridic acid 1-chloro-ethyl ester / 1,2-dichloro-ethane / 16.25 h / 0 - 20 °C
4: triethylamine / dichloromethane / 16 h / 0 - 20 °C
5: ruthenium tetroxide; sodium periodate / water; ethyl acetate / 16 h / 0 - 20 °C
6: acetonitrile / 2 h / 0 - 20 °C
With
sodium periodate; ruthenium tetroxide; carbonochloridic acid 1-chloro-ethyl ester; sodium methylate; triethylamine; N-ethyl-N,N-diisopropylamine; trichlorophosphate;
In
methanol; dichloromethane; water; ethyl acetate; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile;