3-(5-(4-(pyridin-2-yl)phenyl)-1,3,4-oxadiazol-2-yl)-9-hexyl-9H-carbazole

Base Information

Chemical Name:3-(5-(4-(pyridin-2-yl)phenyl)-1,3,4-oxadiazol-2-yl)-9-hexyl-9H-carbazole
CAS No.:1332585-85-9
Molecular Formula:C₃₁H₂₈N₄O
Molecular Weight:472.59
Hs Code.:

Synonyms:3-(5-(4-(pyridin-2-yl)phenyl)-1,3,4-oxadiazol-2-yl)-9-hexyl-9H-carbazole

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Chemical Property of 3-(5-(4-(pyridin-2-yl)phenyl)-1,3,4-oxadiazol-2-yl)-9-hexyl-9H-carbazole

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Technology Process of 3-(5-(4-(pyridin-2-yl)phenyl)-1,3,4-oxadiazol-2-yl)-9-hexyl-9H-carbazole

There total 7 articles about 3-(5-(4-(pyridin-2-yl)phenyl)-1,3,4-oxadiazol-2-yl)-9-hexyl-9H-carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1332585-84-8
3-(1H-tetrazol-5-yl)-9-hexyl-9H-carbazole

: 190850-37-4
4-(pyridin-2-yl)benzoyl chloride

: 1332585-85-9
3-(5-(4-(pyridin-2-yl)phenyl)-1,3,4-oxadiazol-2-yl)-9-hexyl-9H-carbazole

Guidance literature:: With pyridine; for 6h; Reflux; Inert atmosphere;
DOI:10.1016/j.dyepig.2011.04.005

Reference yield:

: 4041-21-8
N-hexylcarbazole

: 1332585-85-9
3-(5-(4-(pyridin-2-yl)phenyl)-1,3,4-oxadiazol-2-yl)-9-hexyl-9H-carbazole

Guidance literature:: Multi-step reaction with 4 steps

1: trichlorophosphate / 6 h / 80 °C / Cooling with ice

2: ammonium hydroxide; iodine / tetrahydrofuran / 1.5 h / 20 °C

3: sodium azide; ammonium chloride / N,N-dimethyl-formamide / 72 h / 120 °C

4: pyridine / 6 h / Reflux; Inert atmosphere

With pyridine; ammonium hydroxide; sodium azide; iodine; ammonium chloride; trichlorophosphate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/j.dyepig.2011.04.005

Reference yield:

: 111-25-1
1-bromo-hexane

: 1332585-85-9
3-(5-(4-(pyridin-2-yl)phenyl)-1,3,4-oxadiazol-2-yl)-9-hexyl-9H-carbazole

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium hydroxide / acetone / 0.5 h

1.2: 10 h

2.1: trichlorophosphate / 6 h / 80 °C / Cooling with ice

3.1: ammonium hydroxide; iodine / tetrahydrofuran / 1.5 h / 20 °C

4.1: sodium azide; ammonium chloride / N,N-dimethyl-formamide / 72 h / 120 °C

5.1: pyridine / 6 h / Reflux; Inert atmosphere

With pyridine; ammonium hydroxide; sodium azide; iodine; ammonium chloride; potassium hydroxide; trichlorophosphate; In tetrahydrofuran; N,N-dimethyl-formamide; acetone;
DOI:10.1016/j.dyepig.2011.04.005