trans/cis-3,4,5-trimethoxybenzoic acid 4-(4-hydroxycyclohexylamino)cyclohexyl ester

Base Information

Chemical Name:trans/cis-3,4,5-trimethoxybenzoic acid 4-(4-hydroxycyclohexylamino)cyclohexyl ester
CAS No.:929548-63-0
Molecular Formula:C₂₂H₃₃NO₆
Molecular Weight:407.507
Hs Code.:

Synonyms:trans/cis-3,4,5-trimethoxybenzoic acid 4-(4-hydroxycyclohexylamino)cyclohexyl ester

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Chemical Property of trans/cis-3,4,5-trimethoxybenzoic acid 4-(4-hydroxycyclohexylamino)cyclohexyl ester

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Technology Process of trans/cis-3,4,5-trimethoxybenzoic acid 4-(4-hydroxycyclohexylamino)cyclohexyl ester

There total 4 articles about trans/cis-3,4,5-trimethoxybenzoic acid 4-(4-hydroxycyclohexylamino)cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 929548-57-2
3,4,5-trimethoxybenzoic acid 4-oxocyclohexyl ester

: 929548-63-0
trans/cis-3,4,5-trimethoxybenzoic acid 4-(4-hydroxycyclohexylamino)cyclohexyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: titanium (IV) isopropoxide / benzene / 3 h / 20 °C

2: 150 mg / NaBH₃CN / ethanol; benzene / 20 h

With titanium(IV) isopropylate; sodium cyanoborohydride; In ethanol; benzene;
DOI:10.1021/jm0614432

Reference yield:

: 4521-61-3
3,4,5-Trimethoxybenzoyl chloride

: 929548-63-0
trans/cis-3,4,5-trimethoxybenzoic acid 4-(4-hydroxycyclohexylamino)cyclohexyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 420 mg / CHCl₃ / 8 h / 60 °C

2: titanium (IV) isopropoxide / benzene / 3 h / 20 °C

3: 150 mg / NaBH₃CN / ethanol; benzene / 20 h

With titanium(IV) isopropylate; sodium cyanoborohydride; In ethanol; chloroform; benzene;
DOI:10.1021/jm0614432

Reference yield:

: 118-41-2
Eudesmic acid

: 929548-63-0
trans/cis-3,4,5-trimethoxybenzoic acid 4-(4-hydroxycyclohexylamino)cyclohexyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: SOCl₂ / 4 h / 80 °C

2: 420 mg / CHCl₃ / 8 h / 60 °C

3: titanium (IV) isopropoxide / benzene / 3 h / 20 °C

4: 150 mg / NaBH₃CN / ethanol; benzene / 20 h

With titanium(IV) isopropylate; thionyl chloride; sodium cyanoborohydride; In ethanol; chloroform; benzene;
DOI:10.1021/jm0614432