[μ-(1,4-phenylenedi-2,1-ethynediyl)]bis(triphenylphosphine)digold

Base Information

Chemical Name:[μ-(1,4-phenylenedi-2,1-ethynediyl)]bis(triphenylphosphine)digold
CAS No.:408495-44-3
Molecular Formula:C₄₆H₃₄Au₂P₂
Molecular Weight:1042.66
Hs Code.:

Synonyms:[μ-(1,4-phenylenedi-2,1-ethynediyl)]bis(triphenylphosphine)digold

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Chemical Property of [μ-(1,4-phenylenedi-2,1-ethynediyl)]bis(triphenylphosphine)digold

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Technology Process of [μ-(1,4-phenylenedi-2,1-ethynediyl)]bis(triphenylphosphine)digold

There total 1 articles about [μ-(1,4-phenylenedi-2,1-ethynediyl)]bis(triphenylphosphine)digold which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 14243-64-2
(triphenylphosphine)gold(I) chloride

: 935-14-8
1,4-diethynylbenzene

: 408495-44-3
[μ-(1,4-phenylenedi-2,1-ethynediyl)]bis(triphenylphosphine)digold

Guidance literature:: With copper(l) iodide; sodium methylate; In methanol; (N2); standard Schlenk technique; Au complex, ligand and CuI were stirred in soln. of CH3ONa in MeOH for 12 h; CH2Cl2 added; filtered through plug of silica; solvent removed (vac.); elem. anal.;
DOI:10.1016/S0022-328X(01)01281-5

Reference yield: 68.0%

: 20224-83-3
PPh₃Au^IC₈H₅

: 408495-44-3
[μ-(1,4-phenylenedi-2,1-ethynediyl)]bis(triphenylphosphine)digold

: ((PPh₃Au)2(C₂N₃))2(C₆H₄)

Guidance literature:: In chloroform; at 20 ℃; for 50h; Inert atmosphere; Schlenk technique; Glovebox;
DOI:10.1039/c5dt00282f

Reference yield: 55.4%

: 408495-44-3
[μ-(1,4-phenylenedi-2,1-ethynediyl)]bis(triphenylphosphine)digold

: 84466-87-5
4-(azidomethyl)benzonitrile

: 4,4'-((4,4'-(1,4-phenylene)bis(5-gold(I)triphenylphosphine-1H-1,2,3-triazole-4,1-diyl))bis(methylene))dibenzonitrile

Guidance literature:: With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In tert-butyl methyl ether; water; tert-butyl alcohol; Inert atmosphere; Schlenk technique;
DOI:10.1021/acs.organomet.9b00291