N-(3,4-dichlorophenyl)-N'-isopropyl-N''-(1-isopropyl-4,5-dihydro-1H-imidazol-2-yl)guanidine hydrochloride

Base Information

Chemical Name:N-(3,4-dichlorophenyl)-N'-isopropyl-N''-(1-isopropyl-4,5-dihydro-1H-imidazol-2-yl)guanidine hydrochloride
CAS No.:1404223-05-7
Molecular Formula:C₁₆H₂₃Cl₂N₅*ClH
Molecular Weight:392.759
Hs Code.:

Synonyms:N-(3,4-dichlorophenyl)-N'-isopropyl-N''-(1-isopropyl-4,5-dihydro-1H-imidazol-2-yl)guanidine hydrochloride

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Chemical Property of N-(3,4-dichlorophenyl)-N'-isopropyl-N''-(1-isopropyl-4,5-dihydro-1H-imidazol-2-yl)guanidine hydrochloride

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Technology Process of N-(3,4-dichlorophenyl)-N'-isopropyl-N''-(1-isopropyl-4,5-dihydro-1H-imidazol-2-yl)guanidine hydrochloride

There total 5 articles about N-(3,4-dichlorophenyl)-N'-isopropyl-N''-(1-isopropyl-4,5-dihydro-1H-imidazol-2-yl)guanidine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 1332704-19-4
1-(3,4-dichlorophenyl)-3-(1-isopropyl-4,5-dihydro-1H-imidazol-2-yl)thiourea

: 75-31-0
isopropylamine

: 1404223-05-7
N-(3,4-dichlorophenyl)-N'-isopropyl-N''-(1-isopropyl-4,5-dihydro-1H-imidazol-2-yl)guanidine hydrochloride

Guidance literature:: With mercury dichloride; In acetonitrile; at 20 ℃; for 0.0833333h; Inert atmosphere;
DOI:10.1021/jm200503s

Reference yield:

: 766449-90-5
1-isopropyl-4,5-dihydro-1H-imidazol-2-ylamine

: 1404223-05-7
N-(3,4-dichlorophenyl)-N'-isopropyl-N''-(1-isopropyl-4,5-dihydro-1H-imidazol-2-yl)guanidine hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 72 h / 20 °C / Inert atmosphere

2: mercury dichloride / acetonitrile / 0.08 h / 20 °C / Inert atmosphere

With triethylamine; mercury dichloride; In dichloromethane; acetonitrile;
DOI:10.1021/jm200503s

Reference yield:

: 19522-67-9
N-isopropylethane-1,2-diamine

: 1404223-05-7
N-(3,4-dichlorophenyl)-N'-isopropyl-N''-(1-isopropyl-4,5-dihydro-1H-imidazol-2-yl)guanidine hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: methanol / 1 h / 0 °C / Inert atmosphere; Reflux

2: triethylamine / dichloromethane / 72 h / 20 °C / Inert atmosphere

3: mercury dichloride / acetonitrile / 0.08 h / 20 °C / Inert atmosphere

With triethylamine; mercury dichloride; In methanol; dichloromethane; acetonitrile;
DOI:10.1021/jm200503s