C₁₈H₁₀ClFN₂O

Base Information

Chemical Name:C₁₈H₁₀ClFN₂O
CAS No.:1367127-68-1
Molecular Formula:C₁₈H₁₀ClFN₂O
Molecular Weight:324.742
Hs Code.:

C<sub>18</sub>H<sub>10</sub>ClFN<sub>2</sub>O

Synonyms:C₁₈H₁₀ClFN₂O

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Chemical Property of C₁₈H₁₀ClFN₂O

Chemical Property:

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Technology Process of C₁₈H₁₀ClFN₂O

There total 6 articles about C₁₈H₁₀ClFN₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 32710-65-9
2,6-dichloro-4-cyanopyridine

: 1355052-34-4
2-(4-(4-fluorophenoxy)phenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1367127-68-1
C₁₈H₁₀ClFN₂O

: 1367127-70-5
C₃₀H₁₈F₂N₂O₂

Guidance literature:: With tetrabutyl ammonium fluoride; palladium bis[bis(diphenylphosphino)ferrocene] dichloride; at 60 ℃; for 2h; Inert atmosphere;

Reference yield:

: 36160-82-4
4-(4-fluorophenoxy)aniline

: 1367127-68-1
C₁₈H₁₀ClFN₂O

: 1367127-70-5
C₃₀H₁₈F₂N₂O₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: sulfuric acid / 1,2-dimethoxyethane; water

1.2: 0.83 h / 0 - 5 °C

1.3: 0.5 h / 0 °C

2.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane / 0.17 h / 20 °C / Inert atmosphere

2.2: 18 h / 90 °C / Inert atmosphere

3.1: tetrabutyl ammonium fluoride / palladium bis[bis(diphenylphosphino)ferrocene] dichloride / 2 h / 60 °C / Inert atmosphere

With sulfuric acid; tetrabutyl ammonium fluoride; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; palladium bis[bis(diphenylphosphino)ferrocene] dichloride; In 1,4-dioxane; 1,2-dimethoxyethane; water;

Reference yield:

: 2561-25-3
4-(4-fluorophenoxy)-1-nitrobenzene

: 1367127-68-1
C₁₈H₁₀ClFN₂O

: 1367127-70-5
C₃₀H₁₈F₂N₂O₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogen / 5%-palladium/activated carbon / methanol / 20 °C / Inert atmosphere

2.1: sulfuric acid / 1,2-dimethoxyethane; water

2.2: 0.83 h / 0 - 5 °C

2.3: 0.5 h / 0 °C

3.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane / 0.17 h / 20 °C / Inert atmosphere

3.2: 18 h / 90 °C / Inert atmosphere

4.1: tetrabutyl ammonium fluoride / palladium bis[bis(diphenylphosphino)ferrocene] dichloride / 2 h / 60 °C / Inert atmosphere

With sulfuric acid; tetrabutyl ammonium fluoride; hydrogen; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; palladium bis[bis(diphenylphosphino)ferrocene] dichloride; 5%-palladium/activated carbon; In 1,4-dioxane; methanol; 1,2-dimethoxyethane; water;