tert-butyl (4-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)phenoxy)dimethylsilane

Base Information

Chemical Name:tert-butyl (4-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)phenoxy)dimethylsilane
CAS No.:1188303-92-5
Molecular Formula:C₁₇H₂₉BO₃Si
Molecular Weight:320.312
Hs Code.:

Synonyms:tert-butyl (4-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)phenoxy)dimethylsilane

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Chemical Property of tert-butyl (4-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)phenoxy)dimethylsilane

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Technology Process of tert-butyl (4-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)phenoxy)dimethylsilane

There total 1 articles about tert-butyl (4-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)phenoxy)dimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 126-30-7
2,2-Dimethyl-1,3-propanediol

: 159191-56-7
(4-((tert-butyldimethylsilyl)oxy)phenyl)boronic acid

: 1188303-92-5
tert-butyl (4-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)phenoxy)dimethylsilane

Guidance literature:: In dichloromethane; at 20 ℃; for 12h;
DOI:10.1021/acs.orglett.9b02236

Reference yield: 90.0%

: 124-38-9,18923-20-1
carbon dioxide

: 1188303-92-5
tert-butyl (4-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)phenoxy)dimethylsilane

: 83405-98-5
4-(tert-butyl-dimethylsilanyloxy)-benzoic acid

Guidance literature:: carbon dioxide; tert-butyl (4-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)phenoxy)dimethylsilane; With [Ni(N,N'-bis[2,6-bis(diphenylmethyl)-4-methylphenyl]imidazole-2-ylidene)(allyl)Cl]; potassium tert-butylate; In toluene; at 100 ℃; for 15h; under 760.051 Torr; Schlenk technique; Inert atmosphere;

With hydrogenchloride; In water; ethyl acetate; toluene; at 20 ℃;
DOI:10.1039/c4cc03650f

Reference yield: 84.0%

: 1188303-92-5
tert-butyl (4-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)phenoxy)dimethylsilane

: 590-86-3
isovaleraldehyde

: 1188303-97-0
1-(4-(tert-butyldimethylsilyloxy)phenyl)-3-methylbutan-1-ol

Guidance literature:: tert-butyl (4-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)phenoxy)dimethylsilane; isovaleraldehyde; With bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; 1,3-bis-(2,6-diisopropylphenyl)-imidazol-2-ylidene; In toluene; at 23 ℃; Inert atmosphere;

With water; In diethyl ether; toluene; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ol9017613