2'-O-(tert-butyl)dimethylsilylinosinyl<2'-P-(2-(p-nitrophenyl)ethyl)><*>5'>-2',3'-di-O-benzoylinosine

Base Information

• Chemical Name: 2'-O-(tert-butyl)dimethylsilylinosinyl<2'-P-(2-(p-nitrophenyl)ethyl)><*>5'>-2',3'-di-O-benzoylinosine
• CAS No.: 85363-71-9
• Molecular Formula: C₄₈H₅₂N₉O₁₆PSi
• Molecular Weight: 1070.05

Synonyms:2'-O-(tert-butyl)dimethylsilylinosinyl<2'-P-(2-(p-nitrophenyl)ethyl)><*>5'>-2',3'-di-O-benzoylinosine

Chemical Property of 2'-O-(tert-butyl)dimethylsilylinosinyl<2'-P-(2-(p-nitrophenyl)ethyl)><*>5'>-2',3'-di-O-benzoylinosine

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 2'-O-(tert-butyl)dimethylsilylinosinyl<2'-P-(2-(p-nitrophenyl)ethyl)><*>5'>-2',3'-di-O-benzoylinosine

There total 18 articles about 2'-O-(tert-butyl)dimethylsilylinosinyl<2'-P-(2-(p-nitrophenyl)ethyl)><*>5'>-2',3'-di-O-benzoylinosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

2'-O-(tert-butyl)dimethylsilyl-5'-O-(o-monomethoxytrityl)inosinyl<2'-P-(2-(p-nitrophenyl)ethyl)><*>5'>-2',3'-di-O-benzoylinosine → 2'-O-(tert-butyl)dimethylsilylinosinyl<2'-P-(2-(p-nitrophenyl)ethyl)><*>5'>-2',3'-di-O-benzoylinosine (85363-71-9)

Guidance literature:

With toluene-4-sulfonic acid; In methanol; dichloromethane; for 0.5h;

Reference yield:

Inosine (58-63-9) → 2'-O-(tert-butyl)dimethylsilylinosinyl<2'-P-(2-(p-nitrophenyl)ethyl)><*>5'>-2',3'-di-O-benzoylinosine (85363-71-9)

Guidance literature:

Multi-step reaction with 5 steps

1: 80 percent

2: benzoylation

3: detritylation

4: 76 percent

DOI:10.1016/S0040-4039(00)85714-7

Reference yield:

tert-butyldimethylsilyl chloride (18162-48-6) → 2'-O-(tert-butyl)dimethylsilylinosinyl<2'-P-(2-(p-nitrophenyl)ethyl)><*>5'>-2',3'-di-O-benzoylinosine (85363-71-9)

Guidance literature:

Multi-step reaction with 5 steps

1: 40 percent / imidazole / pyridine

2: 1.) pyridine

3: oximate

4: 76 percent

With 1H-imidazole; oximate; In pyridine;

DOI:10.1016/S0040-4039(00)85714-7

upstream raw materials:

C₆₈H₆₈N₉O₁₇PSi

2-(4-nitrophenyl)ethanol

2',3'-di-O-benzoylinosine

5'-O-(4-methoxytrityl)inosine

Downstream raw materials:

C₁₁₆H₁₃₂N₁₉O₃₅P₃Si₃

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