N₆-benzoyl-5'-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-2',3'-O-isopropylidene-8-{[(4-methoxyphenyl)diphenylmethoxy]methyl}-N₆-methyladenosine

Base Information

• Chemical Name: N₆-benzoyl-5'-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-2',3'-O-isopropylidene-8-{[(4-methoxyphenyl)diphenylmethoxy]methyl}-N₆-methyladenosine
• CAS No.: 1184837-75-9
• Molecular Formula: C₅₀H₅₉N₅O₇Si
• Molecular Weight: 870.133

Synonyms:N₆-benzoyl-5'-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-2',3'-O-isopropylidene-8-{[(4-methoxyphenyl)diphenylmethoxy]methyl}-N₆-methyladenosine

Chemical Property of N₆-benzoyl-5'-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-2',3'-O-isopropylidene-8-{[(4-methoxyphenyl)diphenylmethoxy]methyl}-N₆-methyladenosine

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Technology Process of N₆-benzoyl-5'-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-2',3'-O-isopropylidene-8-{[(4-methoxyphenyl)diphenylmethoxy]methyl}-N₆-methyladenosine

There total 1 articles about N₆-benzoyl-5'-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-2',3'-O-isopropylidene-8-{[(4-methoxyphenyl)diphenylmethoxy]methyl}-N₆-methyladenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

N(6)-benzoyl-5'-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-2',3'-O-isopropylidene-8-{[(4-methoxyphenyl)diphenylmethoxy]methyl}adenosine (1040239-11-9) + methyl iodide (74-88-4) → N6-benzoyl-5'-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-2',3'-O-isopropylidene-8-{[(4-methoxyphenyl)diphenylmethoxy]methyl}-1-methyladenosine (1184837-76-0) + N6-benzoyl-5'-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-2',3'-O-isopropylidene-8-{[(4-methoxyphenyl)diphenylmethoxy]methyl}-N6-methyladenosine (1184837-75-9)

Guidance literature:

With tetrabutylammomium bromide; sodium hydroxide; In dichloromethane; water; at 25 ℃;

DOI:10.1002/hlca.200900075

Reference yield: 79.0%

N6-benzoyl-5'-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-2',3'-O-isopropylidene-8-{[(4-methoxyphenyl)diphenylmethoxy]methyl}-N6-methyladenosine (1184837-75-9) → N6-benzoyl-5'-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-8-(hydroxymethyl)-2',3'-O-isopropylidene-N6-methyladenosine (1184837-77-1)

Guidance literature:

With triethylsilane; dichloro-acetic acid; In dichloromethane; at 25 ℃;

DOI:10.1002/hlca.200900075

upstream raw materials:

N⁽⁶⁾-benzoyl-5'-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-2',3'-O-isopropylidene-8-{[(4-methoxyphenyl)diphenylmethoxy]methyl}adenosine

methyl iodide

Downstream raw materials:

N₆-benzoyl-5'-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-8-(hydroxymethyl)-2',3'-O-isopropylidene-N₆-methyladenosine

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